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Hyperbranched surfactant and preparation method thereof

A surfactant, hyperbranched technology, applied in chemical instruments and methods, chemical/physical processes, transportation and packaging, etc., can solve the problems of complex process, complex process and high cost of terminal group modification, and achieve the reaction conditions. The effect of mildness, simple preparation process and strong emulsifying ability

Active Publication Date: 2022-03-01
NINGBO FENGCHENG ADVANCED ENERGY MATERIALS RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Usually, a large amount of organic solvents are used in the synthesis of hyperbranched polymers, and the process of terminal group modification is relatively complicated. The overall preparation process is complex, costly, and not environmentally friendly.

Method used

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  • Hyperbranched surfactant and preparation method thereof
  • Hyperbranched surfactant and preparation method thereof
  • Hyperbranched surfactant and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0063] The preparation of embodiment 1 hyperbranched surfactant 1#

[0064] Step (1) Synthesis of hyperbranched polyester amine: Polyethylene glycol (200) diacrylate and N-aminoethylpiperazine are mixed in a reaction vessel with deionized water according to the amount of substance at 1:1 to obtain a solid content of 30% of the reaction solution, the reaction container is sealed, the reaction temperature is 30 ° C, and the reaction time is 6 days under stirring conditions. After the reaction is completed, a hyperbranched polyester amine solution is obtained;

[0065] Step (2) hyperbranched surfactant synthesis: take by weighing 2-acryloyl fatty amino dodecyl sodium dodecylsulfonate by 0.5 times of the amount of substance in step (1) and dissolve in In ionized water, a solution with a solid content of 30% was obtained, which was added to the reaction vessel in step (1) in situ, the reaction vessel was sealed, the reaction temperature was 30°C, and the reaction time was 1d under ...

Embodiment 2

[0066] The preparation of embodiment 2 hyperbranched surfactant 2#

[0067] Step (1) Synthesis of hyperbranched polyester amine: Polyethylene glycol (400) diacrylate and N-aminoethylpiperazine are mixed in a reaction vessel with deionized water according to the amount of substance at 1:1 to obtain a solid content of 30% of the reaction solution, the reaction container is sealed, the reaction temperature is 25 ° C, and the reaction time is 5 days under stirring conditions. After the reaction is completed, a hyperbranched polyester amine solution is obtained;

[0068] Step (2) hyperbranched surfactant synthesis: N-aminoethylpiperazine is weighed 2-acryloyl fatty amino octadecyl sodium sulfonate by 0.5 times of the amount of substance in step (1) and dissolved in In deionized water, a solution with a solid content of 30% was obtained, which was added to the reaction vessel in step (1) in situ, and the reaction vessel was sealed at a reaction temperature of 25°C. Under stirring co...

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Abstract

The invention discloses a hyperbranched surfactant and a preparation method thereof. According to the invention, a hyperbranched polyesteramine polymer with an amino terminal is synthesized, and the amino terminal is subjected to active chain segment modification, so that a hyperbranched surfactant with the hyperbranched polymer as an inner core and an active chain segment as a shell can be obtained. The hyperbranched surfactant provided by the invention has a spatial three-dimensional structure and a unique hole structure, so that the hyperbranched surfactant has good surface / interface activity, thereby having great advantages in the aspects of wetting, washing, emulsifying, compatibilizing and the like. The hyperbranched surfactant is simple in preparation method, environment-friendly in process and excellent in performance.

Description

technical field [0001] The application relates to a surfactant and a preparation method thereof, belonging to the field of surfactants. Background technique [0002] Hyperbranched polymers are homologues of dendritic polymers, which are a type of highly branched three-dimensional macromolecules. , Several layers of branch units and peripheral groups are connected by chemical bonds. Although the structure of hyperbranched polymers is not as perfect as that of dendrimers, its physical and chemical properties are close to those of dendrimers. Hyperbranched polymers have many branch points, the molecular chains are not easy to entangle, the viscosity does not change with the increase of molecular weight, and there are abundant terminal functional groups, which are easy to modify and modify, which is conducive to the synthesis of various functional materials. In addition, the synthesis of dendritic polymers is relatively complicated, and generally requires step-by-step protecti...

Claims

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Application Information

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IPC IPC(8): C09K23/44C09K23/42C08G73/02
CPCC08G73/024
Inventor 崔浩业吴志连陈斌刚张静张侃王耀国
Owner NINGBO FENGCHENG ADVANCED ENERGY MATERIALS RES INST CO LTD
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