Preparation method of low-refractive index nanofiber membrane for alcohol detection
A technology of nanofiber membrane and low refractive index, applied in fiber treatment, fiber chemical characteristics, cellulose/protein conjugated artificial filament, etc., can solve the problems of chemical sensor effectiveness limitation, functional damage, and inability to meet universal applicability
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Embodiment 1
[0032] This embodiment provides a kind of preparation method of the low refractive index nanofiber membrane that is used for alcohol detection, and it comprises the following steps:
[0033] S1. Weigh a certain amount of polyvinyl alcohol and distilled water, put the polyvinyl alcohol and distilled water into the reagent bottle A according to a certain ratio, and then weigh a certain amount of perfluorodecyltriethoxysilane and dissolve it in the above PVA solution In the process, a fluorine-rich PVA solution with a mass concentration of 12% was obtained, and stirred and mixed on a magnetic stirrer for 2 hours to obtain a clear and uniform first spinning precursor solution.
[0034] S2. Weigh a certain amount of N,N-dimethylformamide and acetone, put N,N-dimethylformamide and acetone into the reagent bottle B according to the volume ratio of 7:3 to obtain a clear and uniform total Solvent, then weigh a certain amount of polyvinylidene fluoride-hexafluoroethylene and add it to t...
Embodiment 2
[0038] This embodiment provides a kind of preparation method of the low refractive index nanofiber membrane that is used for alcohol detection, and it comprises the following steps:
[0039] S1. Weigh a certain amount of polyvinyl alcohol and distilled water, put the polyvinyl alcohol and distilled water into the reagent bottle A according to a certain ratio, and then weigh a certain amount of perfluorodecyltriethoxysilane and dissolve it in the above PVA solution In the process, a fluorine-rich PVA solution with a mass concentration of 12% was obtained, and stirred and mixed on a magnetic stirrer for 2 hours to obtain a clear and uniform first spinning precursor solution.
[0040] S2. Weigh a certain amount of N,N-dimethylformamide and acetone, put N,N-dimethylformamide and acetone into the reagent bottle B according to the volume ratio of 7:3 to obtain a clear and uniform total Solvent, then weigh a certain amount of polyvinylidene fluoride-hexafluoroethylene and add it to t...
Embodiment 3
[0044] This embodiment provides a kind of preparation method of the low refractive index nanofiber membrane that is used for alcohol detection, and it comprises the following steps:
[0045] S1. Weigh a certain amount of polyvinyl alcohol and distilled water, put the polyvinyl alcohol and distilled water into the reagent bottle A according to a certain ratio, and then weigh a certain mass of perfluorodecyltriethoxysilane with a concentration of 3%. Dissolve in the above PVA solution to obtain a fluorine-rich PVA solution with a mass concentration of 12%. Stir and mix on a magnetic stirrer for 2 hours to obtain a clear and uniform first spinning precursor solution.
[0046] S2. Weigh a certain amount of N,N-dimethylformamide and acetone, put N,N-dimethylformamide and acetone into the reagent bottle B according to the volume ratio of 7:3 to obtain a clear and uniform total Solvent, then weigh a certain amount of polyvinylidene fluoride-hexafluoroethylene (PVDF-HFP) and add it to...
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