Method for producing biodiesel by combining biological enzyme esterification and supercritical technology
A supercritical technology and biodiesel technology, which is applied in the field of biodiesel production by combining biological enzyme esterification and supercritical technology to achieve the effects of high efficiency and fast reaction process, energy saving and environmental protection in the production process, good economic benefits and social benefits
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[0039] Embodiment 1 The method of combining biological enzyme esterification and supercritical technology to produce biodiesel according to the present invention comprises the following steps:
[0040]The first step, the reaction raw material preparation:
[0041] Add 1000kg of raw material oil into the reaction kettle with stirring function (before the raw material oil enters the reaction kettle through the delivery pump, the temperature can be adjusted to 40~45°C through the heat exchanger), and about 4kg of NaOH solution (concentration 10°C) is added through the metering pump %), adjust the pH value of the raw material oil to 5~7, and then add 2kg of lipase (with an activity of 100,000 units) through a metering pump; mix the raw material oil, NaOH solution and biological enzyme in the reaction kettle, and the mixing time is 3 ~5 minutes;
[0042] The second step, esterification reaction
[0043] After the first step is completed, keep the temperature at 40~45°C, add 130kg...
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