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262results about How to "Post-processing is simple" patented technology

Preparation method of oxidized graphene and sodium alginate composite absorbing material capable of removing ciprofloxacin in aqueous solution

The invention provides a preparation method of an oxidized graphene and sodium alginate composite absorbing material capable of removing ciprofloxacin in an aqueous solution. The preparation method comprises the following steps: dispersing a certain amount of oxidized graphene samples in deionized water, putting the oxidized graphene samples into an ultrasonic cleaner, and performing ultrasonic treatment for 6-10 hours; dissolving a certain amount of sodium alginate into an oxidized graphene solution subjected to ultrasonic treatment, and performing ultrasonic treatment for 20 minutes; dropewise adding the mixed solution into a 0.2mol/L calcium chloride solution by virtue of a peristaltic pump, soaking for 1-3 days, and cleaning with deionized water for 3-4 times, thereby obtaining a sodium alginate and oxidized graphene sphere hydrogel material; and freeze-drying, thereby obtaining oxidized graphene and sodium alginate sphere aerogel. The preparation method is performed under a relatively mild condition, and oxidized graphene is packaged in a sodium alginate network structure by an ion bridge method, so that the nano toxicity of graphene powder is avoided, and a new nano material capable of efficiently absorbing ciprofloxacin antibiotics in the aqueous solution is prepared. The preparation process is simple, easily controllable in condition, low in cost and suitable for large-scale batch production.
Owner:SHANGHAI INST OF TECH

Method for refining long-carbon chain dicarboxylic acid

ActiveCN104496793AMeet the technical requirements of useLess investmentCarboxylic compound separation/purificationEngineeringCarboxylic acid
The invention relates to a method for refining long-carbon chain dicarboxylic acid. A long-chain dicarboxylic acid crude product prepared by a fermentation method is used as a raw material, acetic acid is used as a solvent, and the refining and purification are performed by recrystallization treatment. The method comprises the process steps of bleaching filtration, cooling crystallization, centrifugal separation, centrifugal material washing, secondary centrifugation and drying, and is characterized in that a. the long-chain dicarboxylic acid crude product to be refined does not need to be dried; b. the acetic acid solvent is recycled by an azeotropic distillation method, and isopropyl acetate is used as an azeotropic dehydrating agent; and c. the isopropyl acetate is used as a centrifugal material washing solvent for replacing the acetic acid. The purification method of the long-carbon chain dicarboxylic acid provided by the invention has the advantages of distillation equipment investment conservation, low operating power consumption, good product color, high purity, high refining yield and low production cost, the long-carbon chain dicarboxylic acid to be refined does not need to be dried and dehydrated, and the acetic acid solvent is completely recyclable. The quality of the refined product can meet the technical requirements of use of condensed monomer raw materials used by synthesis of high polymer materials.
Owner:山东广通新材料有限公司

Preparation method of phosphinobenzene compound

The invention relates to a preparation method of a phosphinobenzene compound. The method is characterized in that a bromobenzene compound reacts with magnesium to prepare a Grignard reagent, and the Grignard reagent reacts with a chlorophosphine compound under the catalysis of tetrakis(triphenylphosphine)palladium to obtain the phosphinobenzene compound. The method concretely comprises the following steps: preparing the Grignard reagent from the bromobenzene compound, magnesium chips and an organic solvent under the protection of insert gas, and refluxing for 2-10h; adding tetrakis(triphenylphosphine)palladium at room temperature, stirring for 10min-3h, adding the chlorophosphine compound at room temperature in a dropwise manner, and carrying out a refluxing reaction for 1-10h; and adding an aqueous solution of saturated weakly-acidic and weakly-alkaline salt to the above obtained reaction solution in a dropwise manner in ice-water bath, carrying out liquid separation, removing the solvent from the obtained organic phase, adding an alcohol solvent for crystallizing, and filtering obtained crystals to obtain the phosphinobenzene compound. The preparation method has the advantages of great increase of the preparation yield, simple post-treatment, omitting of the repeated ammonia water washing process, preparation process simplification, and facilitation of large-scale industrial production.
Owner:BEIJING GREENCHEM TECH

Preparation method of zinc oxide microsphere with nanoflower-shaped microstructure

The invention relates to a preparation method of a zinc oxide microsphere with a nanoflower-shaped microstructure. The method comprises the following steps of: (1) preparing a solution, to be specific, preparing a soluble zinc salt into an aqueous solution, and preparing a soluble alkali into an aqueous solution; (2) mixing the solutions, to be specific, mixing the soluble zinc salt aqueous solution with the soluble alkali aqueous solution at the room temperature in the volume ratio of 1:10-10:1, slowly pouring an aqueous solution of a soluble zinc salt into the aqueous solution of the soluble alkali, and stirring to obtain a clarifying solution; and (3) preparing a product, to be specific, pouring a weakly-acid solution into the clarifying solution obtained in the step (2), wherein the volume ratio of the weakly-acid solution to the clarifying solution is 1:10-10:1, stirring to obtain a turbid solution containing a large quantity of products, repeatedly washing with deionized water and absolute ethyl alcohol, and drying in a baking oven to obtain a final product. Compared with the prior art, the method has the advantages of capability of rapidly, easily and conveniently preparing a product under the room temperature condition, high yield, low cost, environmental friendliness, wide raw material selection range and contribution to industrial production.
Owner:SHANGHAI JIAO TONG UNIV

Method for synthesizing o-phenylenediamine from ortho-nitroaniline by virtue of catalytic hydrogenation

The invention provides a method for synthesizing o-phenylenediamine from ortho-nitroaniline by virtue of catalytic hydrogenation. The method comprises the following steps: firstly, adding ortho-nitroaniline and a palladium-carbon catalyst into a high-pressure reaction kettle, introducing nitrogen to exhaust air in the kettle, and then introducing hydrogen to exhaust nitrogen in the kettle; secondly, heating and introducing hydrogen, performing catalytic hydrogenation reduction reaction under the conditions that the temperature is 110 DEG C and the pressure is 1.0MPa, reacting for 7-8 hours, then stopping introducing hydrogen, water-cooling, then filtering to recycle the catalyst, and collecting a filtrate after filtration to obtain o-phenylenediamine. According to the method provided by the invention, a raw material namely ortho-nitroaniline is subjected to direct hydrogenation without using a solvent, so that the consumption of the solvent can be greatly reduced, the after-treatment energy consumption can be saved, and large-sized solvent steaming equipment can be saved; and by adopting the method, a separation process can be simplified, the equipment investment, separation energy consumption, material consumption and environmental pollution can be reduced, and the system productivity and production safety can be improved.
Owner:XIAN CATALYST NEW MATERIALS CO LTD
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