Beer decolorizing film and preparation method thereof

A beer and decolorization technology, applied in the preparation of alcoholic beverages, chemical instruments and methods, membrane technology, etc., can solve problems such as high operating pressure requirements, consumables, solid-liquid separation, etc., to improve swelling resistance, improve osmotic flow Quantity, strong anti-pollution effect

Active Publication Date: 2022-04-12
JIANGSU JIUMO HIGH TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the activated carbon process has the following problems: (1) After decolorization, activated carbon is dissolved in the solution as a solid, and there is a problem of solid-liquid separation, which cannot be completely separated at present, and will leak into beer products; (2) In addition to adsorbing pigment substances, activated carbon is partially Ethanol and a large number of aroma components will also be adsorbed; (3) Activated carbon is easy to form solid waste and is a consumable
In addition, some patented technologies at home and abroad use reverse osmosis and ultrafiltration to treat beer. However, the effect of ultrafiltration membranes on pigment interception is not ideal, and the processing capacity of reverse osmosis membranes is too small, requiring high operating pressure.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] Embodiment 1 (comparative example)

[0034] Dissolve PVA powder in hot water at 85°C to prepare a 5% PVA solution; dissolve PAA powder in hot water at 90°C to prepare a 1% PAA solution; mix the above two solutions at a ratio of 1:1, Stir for 24 hours until uniformly mixed to obtain a hydrophilic coating solution. PEI, NMP and LiCl were formulated into a base film liquid at a weight ratio of 12:60:28, coated on the surface of a non-woven fabric, and then immersed in deionized water at 25°C to prepare a base film. The hydrophilic coating solution is applied by slit extrusion coating method, the solution extrusion rate is 0.8mL / min, coated on the surface of the PEI base film, and placed in an oven at 130°C for interfacial polymerization reaction for 4 hours to obtain a non-blocking solution And the PVA / PAA / PEI beer decolorization composite film prepared by the method without cross-linking agent.

Embodiment 2

[0035] Embodiment 2 (comparative example)

[0036] Dissolve PVA powder in hot water at 90°C to prepare a 7% PVA solution; dissolve PAA powder in hot water at 90°C to prepare a 2% PAA solution; mix the above two solutions at a ratio of 1:3, Stir for 24 hours until uniformly mixed to obtain a hydrophilic coating solution. PEI, NMP and LiCl were formulated into a base film liquid at a weight ratio of 15:65:20, coated on the surface of a non-woven fabric, and then immersed in deionized water at 25°C to prepare a base film. The hydrophilic coating solution is applied by slit extrusion coating method, the solution extrusion rate is 1mL / min, coated on the surface of the PEI base film, and placed in an oven at 140°C for interfacial polymerization reaction for 6 hours to obtain a non-blocking solution and PVA / PAA / PEI beer decolorization composite film prepared by cross-linking agent-free method.

Embodiment 3

[0037] Embodiment 3 (comparative example)

[0038] Dissolve PVA powder in 95°C hot water to prepare 8% PVA solution; dissolve PAA powder in 90°C hot water to prepare 3% PAA solution; mix the above two solutions in a ratio of 1:5, Stir for 24 hours until uniformly mixed to obtain a hydrophilic coating solution. PEI, NMP and LiCl were formulated into a base film solution at a weight ratio of 20:70:10, coated on the surface of a non-woven fabric, and then immersed in deionized water at 25°C to prepare a base film. The hydrophilic coating solution is applied by slit extrusion coating method, the solution extrusion rate is 1.5mL / min, coated on the surface of the PEI base film, placed in an oven at 150°C for interfacial polymerization reaction for 8 hours, and a non-blocking solution is obtained And the PVA / PAA / PEI beer decolorization composite film prepared by the method without cross-linking agent.

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PUM

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Abstract

The invention discloses a beer decolorizing membrane and a preparation method thereof.The beer decolorizing membrane is prepared by taking a mixed solution of PVA, PAA and a cross-linking agent as a hydrophilic membrane coating solution, a mixed solution of gamma-aminopropyltriethoxysilane, water and ethyl alcohol as a hole blocking solution and a non-woven fabric coated with a mixed solution of PEI, NMP and LiCl as a base membrane, immersing the base membrane into the hole blocking solution, and carrying out vacuum drying to obtain the beer decolorizing membrane. And then coating the hydrophilic coating liquid on the surface, and carrying out polymerization reaction. The prepared beer decolorizing membrane is good in hydrophilicity, large in flux and high in pollution resistance, pigments, residual sugar, protein, amino acid and a small amount of other macromolecular flavor components in beer can be effectively intercepted, colorless and transparent beer with the unchanged alcoholic strength is prepared, the colored beer which does not penetrate through the membrane can be sold as low-alcohol beer after being diluted and subjected to alcohol reduction, and the method is suitable for popularization and application. Therefore, the maximum resource utilization of the raw beer is realized.

Description

technical field [0001] The invention relates to the technical field of membrane material preparation, in particular to a beer decolorization membrane and a preparation method thereof. Background technique [0002] Since the birth of beer, it has been generally divided into light yellow beer, dark beer and dark beer according to its color. The most general on the market at present is light yellow beer, although the method of beer production is different, and kind is also more, its color and local flavor are all basically the same, thereby make light yellow beer become the beer beverage kind that is widely accepted by people. In recent years, transparent cola, coffee and beer have become more and more popular. It is generally believed that one of the reasons for the popularity of transparent beverages is the demand for health. This type of beverage product is easier to give consumers the impression of no burden and no calories, caters to the trend of healthy eating in recent ...

Claims

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Application Information

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IPC IPC(8): B01D69/12B01D71/38B01D71/40B01D67/00C12H1/056C12H1/07D06M15/333D06M15/263D06M13/513D06M15/61D06M11/13
Inventor 丁晓斌金万勤邢卫红孙雪飞戴萍萍王成
Owner JIANGSU JIUMO HIGH TECH CO LTD
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