Organic optical nonlinear chromophore based on double-donor structure as well as synthesis method and application of organic optical nonlinear chromophore
An optical nonlinear and chromophore technology, applied in the field of organic optical nonlinear chromophore and its synthesis, can solve the problem of inability to further modify functional groups, and achieve the effect of strong electron donor strength
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[0056] The present invention is further described in conjunction with the following examples.
[0057] The embodiment of the present invention relates to four kinds of organic optical nonlinear chromophores BLD1-4 based on the double-donor structure, and its structure is shown in the attached Figure 2-5 , the chromophore BLD1-4 shows good solubility in common organic solvents, such as ethyl acetate, ethanol and acetone etc., its synthetic method comprises the following steps:
[0058] S1. Add 4,4-difluorobenzophenone (compound (1)) (10.0 g, 46.8 mol) and 2-(ethylamino) ethanol (20.4 g, 229 mmol) to a 500 mL circle equipped with a reflux condenser Bottom flask, and reacted at 180°C under a nitrogen atmosphere for 2d. After the reaction was completed, the mixture was cooled, and the aqueous layer was extracted with ethyl acetate and water, and then the water was removed. Using ethyl acetate / ethanol as a developing solvent, the column chromatography Purify, and then remove resi...
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