Preparation method of ultraviolet aging resistant textile fabric added with attapulgite

Abstract

The invention belongs to the technical field of textile fabrics, and particularly relates to a preparation method of an attapulgite-added anti-ultraviolet aging textile fabric. According to the preparation method, a composite material of attapulgite loaded nano CeO2 and nano ZnO is arranged on cotton fibers, so that the anti-ultraviolet aging textile fabric is prepared. According to the preparation method, not only can the prepared fabric have good mechanical properties, but also the fabric can have lasting and excellent ultraviolet aging resistance. Operation is simple and easy to control. The raw materials are nontoxic and have no carcinogenic effect, the prepared anti-ultraviolet aging fabric is woven by wrapping the surface of the fiber with the anti-ultraviolet aging agent, and the fabric has good anti-ultraviolet aging performance in all directions.

Description

technical field

[0001] The invention belongs to the technical field of textile fabrics, and in particular relates to a preparation method of attapulgite anti-ultraviolet aging textile fabrics. Background technique

[0002] With the rapid development of the economy, people's material living standards continue to improve, the original single and monotonous textiles can no longer meet the development of the times and people's needs. More and more people's requirements for textiles are no longer limited to basic properties such as warmth, breathability, and comfort, and they also hope that they have special functions such as anti-ultraviolet aging and antibacterial. Therefore, it is necessary to develop new multifunctional textile fabrics to meet the urgent needs of modern people.

[0003] Attapulgite is a natural one-dimensional nanomaterial mineral with a special fibrous crystal structure. It is known as the "king of thousands of soils" and has high practical and scientific r...

Examples

Embodiment 1

[0023] A preparation method of adding attapulgite anti-ultraviolet aging textile fabric, the specific steps are as follows:

[0024] (1) Preparation of zinc and cerium composite carbonate: adding 50 ml of zinc nitrate solution with a concentration of 2 mol / L and 104 ml of a cerium sulfate solution with a concentration of 0.5 mol / L into the reactor, stirring evenly, and warming up to 60 ° C, While stirring, add 152 ml of potassium carbonate solution with a concentration of 1 mol / L, after adding, continue to keep stirring for 2 hours, filter, and wash with deionized water until the conductivity of the filtrate is 60 μs / cm, dry and pulverize to obtain zinc and cerium. Complex carbonate.

[0025] (2) Preparation of finishing solution: add 100g of polyethylene glycol 400, 100g of glycerol and 800g of deionized water to the reaction kettle to prepare a mixed solution, and the zinc and cerium composite carbonate prepared in step (1), 48g of attapulgite The stone was added to the mix...

Embodiment 2

[0029] A preparation method of adding attapulgite anti-ultraviolet aging textile fabric, the specific steps are as follows:

[0030] (1) Preparation of zinc and cerium composite carbonate: adding 400ml of zinc sulfate solution with a concentration of 0.5mol / L and 25ml of a cerium nitrate solution with a concentration of 2mol / L into the reactor, stirring evenly, and warming up to 80°C, While stirring, add 113 ml of sodium bicarbonate solution with a concentration of 2 mol / L, after adding, continue to keep stirring for 1 h, filter, and wash with deionized water until the conductivity of the filtrate is 90 μs / cm, dry, pulverize, and obtain zinc, Cerium composite carbonate.

[0031] (2) Preparation of finishing liquid: 150g of polyethylene glycol 400, 150g of glycerol and 700g of deionized water were added to the reaction kettle to prepare a mixed solution, and the zinc, cerium composite carbonate, 24g attapulgite prepared in step (1) The stone was added to the mixed solution and...

Embodiment 3

[0035] A preparation method of adding attapulgite anti-ultraviolet aging textile fabric, the specific steps are as follows:

[0036] (1) Preparation of zinc and cerium composite carbonate: add 100 ml of zinc chloride solution with a concentration of 1.5 mol / L and 46 ml of a cerium chloride solution with a concentration of 1.5 mol / L into the reactor, stir evenly, and heat up to 70°C, while stirring, add 123ml of sodium carbonate solution with a concentration of 1.5mol / L, after adding, continue to keep stirring for 1.5h, filter, and wash with deionized water until the conductivity of the filtrate is 70μs / cm, dry, pulverize, Preparation of zinc, cerium composite carbonate.

[0037] (2) Preparation of finishing solution: 150g of polyethylene glycol 400, 100g of glycerol and 750g of deionized water were added to the reaction kettle to prepare a mixed solution, and the zinc and cerium composite carbonate prepared in step (1), 32g of attapulgite The stone was added to the mixed solu...

technical field

[0001] The invention belongs to the technical field of textile fabrics, and in particular relates to a preparation method of attapulgite anti-ultraviolet aging textile fabrics. Background technique

[0002] With the rapid development of the economy, people's material living standards continue to improve, the original single and monotonous textiles can no longer meet the development of the times and people's needs. More and more people's requirements for textiles are no longer limited to basic properties such as warmth, breathability, and comfort, and they also hope that they have special functions such as anti-ultraviolet aging and antibacterial. Therefore, it is necessary to develop new multifunctional textile fabrics to meet the urgent needs of modern people.

[0003] Attapulgite is a natural one-dimensional nanomaterial mineral with a special fibrous crystal structure. It is known as the "king of thousands of soils" and has high practical and scientific r...

Examples

Embodiment 1

[0023] A preparation method of adding attapulgite anti-ultraviolet aging textile fabric, the specific steps are as follows:

[0024] (1) Preparation of zinc and cerium composite carbonate: adding 50 ml of zinc nitrate solution with a concentration of 2 mol / L and 104 ml of a cerium sulfate solution with a concentration of 0.5 mol / L into the reactor, stirring evenly, and warming up to 60 ° C, While stirring, add 152 ml of potassium carbonate solution with a concentration of 1 mol / L, after adding, continue to keep stirring for 2 hours, filter, and wash with deionized water until the conductivity of the filtrate is 60 μs / cm, dry and pulverize to obtain zinc and cerium. Complex carbonate.

[0025] (2) Preparation of finishing solution: add 100g of polyethylene glycol 400, 100g of glycerol and 800g of deionized water to the reaction kettle to prepare a mixed solution, and the zinc and cerium composite carbonate prepared in step (1), 48g of attapulgite The stone was added to the mix...

Embodiment 2

[0029] A preparation method of adding attapulgite anti-ultraviolet aging textile fabric, the specific steps are as follows:

[0030] (1) Preparation of zinc and cerium composite carbonate: adding 400ml of zinc sulfate solution with a concentration of 0.5mol / L and 25ml of a cerium nitrate solution with a concentration of 2mol / L into the reactor, stirring evenly, and warming up to 80°C, While stirring, add 113 ml of sodium bicarbonate solution with a concentration of 2 mol / L, after adding, continue to keep stirring for 1 h, filter, and wash with deionized water until the conductivity of the filtrate is 90 μs / cm, dry, pulverize, and obtain zinc, Cerium composite carbonate.

[0031] (2) Preparation of finishing liquid: 150g of polyethylene glycol 400, 150g of glycerol and 700g of deionized water were added to the reaction kettle to prepare a mixed solution, and the zinc, cerium composite carbonate, 24g attapulgite prepared in step (1) The stone was added to the mixed solution and...

Embodiment 3

[0035] A preparation method of adding attapulgite anti-ultraviolet aging textile fabric, the specific steps are as follows:

[0036] (1) Preparation of zinc and cerium composite carbonate: add 100 ml of zinc chloride solution with a concentration of 1.5 mol / L and 46 ml of a cerium chloride solution with a concentration of 1.5 mol / L into the reactor, stir evenly, and heat up to 70°C, while stirring, add 123ml of sodium carbonate solution with a concentration of 1.5mol / L, after adding, continue to keep stirring for 1.5h, filter, and wash with deionized water until the conductivity of the filtrate is 70μs / cm, dry, pulverize, Preparation of zinc, cerium composite carbonate.

[0037] (2) Preparation of finishing solution: 150g of polyethylene glycol 400, 100g of glycerol and 750g of deionized water were added to the reaction kettle to prepare a mixed solution, and the zinc and cerium composite carbonate prepared in step (1), 32g of attapulgite The stone was added to the mixed solu...

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