Starch film-forming composition and application thereof in soft capsule
A composition and a technology for soft capsules, which are applied in the field of medicine and dietary supplement manufacturing, can solve problems such as large differences in gel properties, poor soft capsule molding performance, easy pre-gelation, etc., and achieve simple ingredients and meet industrial production requirements. Effect
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[0046] The starch film-forming composition of the present invention can be prepared into soft capsule shells by conventional techniques. For example, the preparation method may include: sol, pelletizing and drying steps. The sol step may include premixing and dispersing the first gellan gum, the second gellan gum and the plasticizer uniformly, adding to an appropriate amount of water with stirring, heating and stirring at 60-98° C. until the gellan gum is dissolved; adding starch, and continuing Heating and stirring at 60-98° C. until the starch dissolves; removing the air bubbles to obtain a glue solution. The pill pressing step may include using a soft capsule production line to transport the glue into the plastic box of the soft capsule filling machine, and the glue is cooled on the surface of the drum to form a rubber, which is compressed and formed by packaging and filling, and can be further shaped in a rotating cage. The prepared soft capsule shells were tested to be e...
Embodiment 1-7
[0092] According to the formulation composition of Table 2, Table 3 and Table 4 and according to the preparation method of the soft capsule skin above, the soft capsule skins of Examples 1-7 were prepared and the capsule skins of Comparative Examples 1-10 were prepared, and the soft capsule skins were determined as described above. Capsule skin strength, toughness and molding adhesion index and enteric solubility.
[0093] Table 2: Film-forming composition formulations and effect measurements of Examples 1-7
[0094]
[0095] √ not cracked, × cracked, / not tested.
[0096] Table 3: Film-forming composition formulation and effect measurement of Comparative Examples 1-5
[0097]
[0098] √ not cracked, × cracked, / not tested.
[0099] Table 4: Film-forming composition formulation and effect measurement of Comparative Examples 6-10
[0100]
[0101] According to Table 2, Table 3 and Table 4, when the comprehensive evaluation is greater than 3, the molding performanc...
Embodiment 8-14
[0106] According to the formula composition of Table 6 and according to the preparation method of the above soft capsule skin, the soft capsule skins of Examples 8-14 were prepared, and the soft capsule skin strength, toughness and molding adhesion index and enteric solubility were determined as described above.
[0107] Softgels were prepared with the ingredients and amounts described in Table 6, and tested and scored. The measurement results are shown in Table 6.
[0108] Table 6: Film-forming composition formulations and tested effects of Example 3 and Examples 8-14.
[0109]
[0110] √ means no rupture × means rupture; USP refers to USP disintegration time limit; in simulated gastric juice (1h); in simulated intestinal juice (1h); European Pharmacopoeia refers to European Pharmacopoeia disintegration time limit; in 0.1M hydrochloric acid (2h); in phosphate buffer pH 6.8 (1h)
[0111] Examples 8-14 illustrate the preparation of soft capsules containing two kinds of p...
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