Modified acrylic UV curing packaging adhesive and preparation method and application thereof
A technology of acrylic and encapsulation glue, applied in the direction of adhesives, non-polymer adhesive additives, adhesive types, etc., can solve the problems of insufficient light source light, time-consuming assembly, light leakage, etc., to ensure the consistency of curing, Improved sealing effect and broad application prospects
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Embodiment 1
[0029] Add 2,6-di-tert-butyl-p-cresol, hydroquinone, stannous octoate and HMDI to hydroxyl-terminated liquid polybutadiene, react at 70°C; then add HEA, IBOA, IBOMA and HEMA at 75°C reaction to obtain hydroxyl terminated liquid polybutadiene modified acrylic resin;
[0030] 20g of IBOA, 15g of acrylic resin, 50g of the above-mentioned hydroxyl-terminated liquid polybutadiene-modified acrylic resin and 2g of silane coupling agent KH560 were stirred at 400rad / min with 3g of fumed silica A200, 10g of silica T804, 3g Photoinitiator 184 and 3g photoinitiator TPO were stirred at 200 rad / min, passed the inspection, packaged, and stored at 15° C. to obtain a modified acrylic UV-curable encapsulant.
Embodiment 2
[0032] Add 2,6-di-tert-butyl-p-cresol, hydroquinone, stannous octoate and HMDI to the hydroxyl-terminated liquid polybutadiene, and react at 60 °C; then add HEA and IBOMA to react at 70 °C to obtain end- Hydroxy liquid polybutadiene modified acrylic resin;
[0033] 15g of IBOMA, 10g of acrylic resin, 45g of the above-mentioned hydroxyl-terminated liquid polybutadiene-modified acrylic resin and 1g of silane coupling agent KH570 were mixed with 1g of fumed silica A200, 5g of silica T804, 1g of light after stirring at 300rad / min. Initiator 184 and 3 g of photoinitiator 369 were stirred at 200 rad / min, passed the inspection, packaged, and stored at 10° C. to obtain a modified acrylic UV-curable encapsulant.
Embodiment 3
[0035] Add 2,6-di-tert-butyl-p-cresol, hydroquinone, stannous octoate and HMDI to the hydroxyl-terminated liquid polybutadiene, and react at 80 °C; then add IBOMA and HEMA to react at 80 °C to obtain the terminal Hydroxy liquid polybutadiene modified acrylic resin;
[0036] 25g HEMA, 20g acrylic resin, 60g above-mentioned hydroxyl-terminated liquid polybutadiene modified acrylic resin and 4g silane coupling agent KH570 were mixed with 4g fumed silica (TS720), 15g silica T804, 5g after stirring at 300rad / min. Photoinitiator 907) and 4g of photoinitiator 369 were stirred at 200 rad / min, passed the inspection, packaged separately, and stored at 25°C to obtain a modified acrylic UV-curable encapsulant.
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