Calcium sulfonate-based compound grease for high-temperature long-life low-noise bearing and preparation method of calcium sulfonate-based compound grease
A technology with calcium sulfonate and long life, applied in the directions of lubricating composition, rolling resistance optimization, road transportation emission reduction, etc., can solve the problems of shortening bearing life, motor stability, reducing working life, uncoordinated action, etc. Avoid environmental pollution and injury to operators, reduce energy consumption and production costs, and use a wide temperature range
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Embodiment 1
[0035] A calcium sulfonate-based composite grease for high temperature, long life and low noise is prepared through the following steps:
[0036] A) Weigh by weight: 24 parts of high base number sulfonic acid calcium salt (TBN=400), 1060 parts of synthetic base oil PAO, 4 parts of phase inversion agent (0.2 part of ethylene glycol, 0.5 part of acetic acid, dodecylbenzene 1.3 parts of sulfonic acid and 2 parts of water), 3 parts of polyurea powder, 1.5 parts of ethylene-propylene copolymer, 2.5 parts of odorless vulcanized olefin, 3 parts of molybdenum diisooctyl dithiocarbamate, 0.5 parts of rust inhibitor T705 , 1 part of organic amine antioxidant, 0.5 part of colloidal structure stabilizer (dodecanol);
[0037] B) using synthetic base oil PAO10 as base oil;
[0038] C) drop the mixture of overbased sulfonic acid calcium salt, synthetic base oil PAO10 and phase inversion agent into the reactor, stir evenly, be warming up to 75~90 ℃, constant temperature 90~120min, complete cal...
Embodiment 2
[0042] A calcium sulfonate-based composite grease for high temperature, long life and low noise is prepared through the following steps:
[0043] A) Weigh in parts by weight: 22 parts of high base number sulfonic acid calcium salt (TBN=400), 61 parts of synthetic base oil trimethylolpropane oleate TMPTO, 4.5 parts of phase inversion agent (0.2 part of propylene glycol, 0.5 part of acetic acid) parts, 1.3 parts of dodecylbenzene sulfonic acid and 2.5 parts of water), 3.5 parts of polyurea powder, 1.5 parts of ethylene-propylene copolymer, 2.5 parts of odorless sulfurized olefin, 3 parts of molybdenum diisooctyl dithiophosphate, anti- Rust agent T7050.5 parts, organic amine antioxidant 1 part, colloidal structure stabilizer (alkene anhydride) 0.5 part;
[0044] B) using synthetic base oil trimethylolpropane oleate TMPTO as base oil;
[0045] C) drop the mixture of overbase number sulfonic acid calcium salt, synthetic base oil trimethylolpropane oleate TMPTO and phase inversion ...
Embodiment 3
[0049] A calcium sulfonate-based composite grease for high temperature, long life and low noise is prepared through the following steps:
[0050] A) Weigh by weight: 23 parts of high base number sulfonic acid calcium salt (TBN=400), 61 parts of synthetic palm oil, 3 parts of phase inversion agent (0.2 part of ethylene glycol, 0.3 part of acetic acid, dodecylbenzene 0.8 parts of sulfonic acid and 1.7 parts of water), 5 parts of polyurea powder, 1.5 parts of ethylene-propylene copolymer, 2.5 parts of odorless vulcanized olefin, 2 parts of molybdenum diisooctyl dithiophosphate, 0.5 parts of rust inhibitor T705, 1 part of phenolic antioxidant, 0.5 part of colloidal structure stabilizer (adipic acid);
[0051] B) using the synthetic base oil palm oil as the base oil;
[0052] C) drop the mixture of overbased sulfonic acid calcium salt, synthetic base oil palm oil and phase inversion agent into the reactor, stir evenly, be warming up to 75~90 ℃, constant temperature 90~120min, comp...
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