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Calcium sulfonate-based compound grease for high-temperature long-life low-noise bearing and preparation method of calcium sulfonate-based compound grease

A technology with calcium sulfonate and long life, applied in the directions of lubricating composition, rolling resistance optimization, road transportation emission reduction, etc., can solve the problems of shortening bearing life, motor stability, reducing working life, uncoordinated action, etc. Avoid environmental pollution and injury to operators, reduce energy consumption and production costs, and use a wide temperature range

Pending Publication Date: 2022-08-09
BAOJI UNIV OF ARTS & SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the use of mineral base oils, this type of low-noise bearing grease is greatly compromised in some physical and chemical indicators other than rust removal and anti-rust performance
If the bearing life can only reach 200 hours, it will be difficult to test the starting and running torque at -20°C
The operating temperature of this type of grease is generally -20 to 120°C. When used at a high temperature above 150°C, the base oil will evaporate too quickly and the loss will be serious, which will greatly shorten the service life of the bearing.
In addition, if the particles enter the working area, they will damage the friction pair and reduce the working life
Low-noise grease can eliminate bearing noise by removing impurity particles or pollutants. These impurities or pollutants cause bearings to be scratched or shaft sleeves to be impacted. If the impurity content is too large, under the same working conditions, Interfere with the normal operation of moving parts, making their movements uncoordinated
This may shorten the life of the bearings and the stability of the motor

Method used

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  • Calcium sulfonate-based compound grease for high-temperature long-life low-noise bearing and preparation method of calcium sulfonate-based compound grease
  • Calcium sulfonate-based compound grease for high-temperature long-life low-noise bearing and preparation method of calcium sulfonate-based compound grease
  • Calcium sulfonate-based compound grease for high-temperature long-life low-noise bearing and preparation method of calcium sulfonate-based compound grease

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0035] A calcium sulfonate-based composite grease for high temperature, long life and low noise is prepared through the following steps:

[0036] A) Weigh by weight: 24 parts of high base number sulfonic acid calcium salt (TBN=400), 1060 parts of synthetic base oil PAO, 4 parts of phase inversion agent (0.2 part of ethylene glycol, 0.5 part of acetic acid, dodecylbenzene 1.3 parts of sulfonic acid and 2 parts of water), 3 parts of polyurea powder, 1.5 parts of ethylene-propylene copolymer, 2.5 parts of odorless vulcanized olefin, 3 parts of molybdenum diisooctyl dithiocarbamate, 0.5 parts of rust inhibitor T705 , 1 part of organic amine antioxidant, 0.5 part of colloidal structure stabilizer (dodecanol);

[0037] B) using synthetic base oil PAO10 as base oil;

[0038] C) drop the mixture of overbased sulfonic acid calcium salt, synthetic base oil PAO10 and phase inversion agent into the reactor, stir evenly, be warming up to 75~90 ℃, constant temperature 90~120min, complete cal...

Embodiment 2

[0042] A calcium sulfonate-based composite grease for high temperature, long life and low noise is prepared through the following steps:

[0043] A) Weigh in parts by weight: 22 parts of high base number sulfonic acid calcium salt (TBN=400), 61 parts of synthetic base oil trimethylolpropane oleate TMPTO, 4.5 parts of phase inversion agent (0.2 part of propylene glycol, 0.5 part of acetic acid) parts, 1.3 parts of dodecylbenzene sulfonic acid and 2.5 parts of water), 3.5 parts of polyurea powder, 1.5 parts of ethylene-propylene copolymer, 2.5 parts of odorless sulfurized olefin, 3 parts of molybdenum diisooctyl dithiophosphate, anti- Rust agent T7050.5 parts, organic amine antioxidant 1 part, colloidal structure stabilizer (alkene anhydride) 0.5 part;

[0044] B) using synthetic base oil trimethylolpropane oleate TMPTO as base oil;

[0045] C) drop the mixture of overbase number sulfonic acid calcium salt, synthetic base oil trimethylolpropane oleate TMPTO and phase inversion ...

Embodiment 3

[0049] A calcium sulfonate-based composite grease for high temperature, long life and low noise is prepared through the following steps:

[0050] A) Weigh by weight: 23 parts of high base number sulfonic acid calcium salt (TBN=400), 61 parts of synthetic palm oil, 3 parts of phase inversion agent (0.2 part of ethylene glycol, 0.3 part of acetic acid, dodecylbenzene 0.8 parts of sulfonic acid and 1.7 parts of water), 5 parts of polyurea powder, 1.5 parts of ethylene-propylene copolymer, 2.5 parts of odorless vulcanized olefin, 2 parts of molybdenum diisooctyl dithiophosphate, 0.5 parts of rust inhibitor T705, 1 part of phenolic antioxidant, 0.5 part of colloidal structure stabilizer (adipic acid);

[0051] B) using the synthetic base oil palm oil as the base oil;

[0052] C) drop the mixture of overbased sulfonic acid calcium salt, synthetic base oil palm oil and phase inversion agent into the reactor, stir evenly, be warming up to 75~90 ℃, constant temperature 90~120min, comp...

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Abstract

The invention discloses calcium sulfonate-based complex grease for a high-temperature long-service-life low-noise bearing and a preparation method of the calcium sulfonate-based complex grease, and belongs to the technical field of lubricating grease preparation. The complex grease consists of the following components in parts by weight: 60-75 parts of synthetic base oil; 20 to 35 parts of high base number sulfonate; 3-6 parts of a phase inversion agent; 3-8 parts of polyurea powder; 1-3 parts of a viscosity index improver, 1.5-4 parts of an anti-wear reagent at extreme pressure, 2-5 parts of an antifriction agent, 0.5-2 parts of an antirust agent, 0.5-2 parts of an antioxidant and 0.5-2 parts of a colloid structure stabilizer; the bearing grease with high dropping point, long service life and low noise is prepared through phase inversion, refining, blending and other processes. The calcium sulfonate-based grease is compounded with the polyurea lubricating grease, so that the soap content of the calcium sulfonate-based lubricating grease is reduced, the service life of a high-temperature bearing is remarkably prolonged, abrasion and equipment failure are reduced, and the use cost is reduced; the lubricating oil is suitable for lubricating and protecting bearings of household appliances, office equipment, precise instruments and various industrial machines which require low noise, rust prevention and long service life (even lifelong lubrication); the motor bearing lubrication device is also suitable for bearing lubrication on scooters, roller skates and bags, and can meet noise reduction, lubrication and protection of other small and medium-sized motor bearings.

Description

technical field [0001] The invention belongs to the technical field of grease preparation, and in particular relates to a calcium sulfonate-based composite grease for high temperature, long life and low noise bearings and a preparation method thereof. Background technique [0002] Low-noise grease is a fully purified grease. If impurities and contaminants enter the bearing or load-bearing parts, it may cause damage to these parts, while low-noise bearing grease has good noise reduction performance, which can effectively reduce The vibration value of the bearing meets the lubrication requirements of long life, low noise and low starting torque. In 2020, the total domestic production of bearings will reach 8 billion sets, each set of bearings is calculated as 0.5g according to the minimum grease filling amount, the consumption of bearing grease will reach 40,000 tons, and the high-end low-noise bearings are calculated as 160 million sets, with high performance and low noise. ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/00C10N30/06C10N30/12C10N30/08C10N40/02C10N50/10
CPCC10M169/00C10N2030/06C10N2030/12C10N2030/08C10N2050/10C10N2040/02C10N2030/68C10N2030/76C10M2219/046C10M2217/0456C10M2207/2835C10M2207/022C10M2207/122C10M2219/044C10M2205/022C10M2205/024C10M2219/082C10M2201/085C10N2010/04C10N2010/12Y02T10/86
Inventor 罗海棠谢龙凡明锦文平
Owner BAOJI UNIV OF ARTS & SCI