Producing process and technology for electronic grade water by intergrated film process

A production process and integrated membrane technology, applied in the field of ultrapure water production technology and process, can solve the problems of low water utilization rate, inability to guarantee qualified water particles of the product, high investment cost, and achieve the effect of ensuring service life

Inactive Publication Date: 2003-04-09
TIANJIN UNIV
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Problems solved by technology

[0017] Second, the equipment investment of the first-level pure water system is too high, and the water utilization rate is low
Although the two-stage reverse osmosis can greatly reduce the burden on the subsequent ion exchange column, the investment cost of the system is too high, and the water utilization rate of the water production system is low
Generally, the total water utilization rate of two-stage reverse osmosis does not exceed 35%.
[0019] 3. Terminal fine treatment still cannot fully meet the requirements
At present, the terminal treatment method of 0.1 μm UF-UV (ultraviolet light)-0.04 μm UF is mostly used, but for the production of integrated circuits with an integration level exceeding 64 MDRAM, it is still impossible to ensure that the indicators such as particles in the product water are qualified

Method used

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  • Producing process and technology for electronic grade water by intergrated film process
  • Producing process and technology for electronic grade water by intergrated film process

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Embodiment Construction

[0051] figure 1 In the process shown, the sand filter-ultrafiltration-activated carbon-security filtration-nanofiltration pretreatment removes suspended solids, particles, pigments, turbidity, organic matter, colloids, microorganisms, calcium and magnesium hardness ions and 50-70 % Salt, the ultrafiltration uses a polyethersulfone ultrafiltration membrane with a molecular weight cut-off of 20,000 to 50,000 Daltons, and the nanofiltration uses an aromatic polyamide ESNAl membrane. Reverse osmosis removes ionic and non-ionic (organic matter, particles, etc.) impurities in the pretreated water. If necessary, adjust the pH between NF and RO, adjust the pH value of the RO inlet water to weakly alkaline, such as pH 9.5, in order to effectively remove TOC and CO 2 And SiO 2 . The RO membrane used is an aromatic polyamide CPA-ULTRAPURE membrane.

[0052] The reverse osmosis pure water tank is protected by nitrogen to avoid secondary air pollution. In addition, fill the water tank with pr...

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Abstract

In the production process, tap water as material water is treated in four parts including pre-treatment unit, the first water purifying system, the second water purifying system and the end film filtering treatment system to prepare electronic level super-pure water. For the treating process, the pre-treatment unit includes sand filtering, superfiltering, active carbon adsorption and nanofiltering; the first water purifying system consists of reverse osmosis, film deairing, electrically deionizing, selective ion exchange resin to eliminate boron impurity and other units; the second water purifying sytem consists of ultraviolet lamp oxidation and polishing mixed bed resin; and the end film filtering treatment is polished reverse osmosis film treatment. The water purifying system has high efficiency, and low cost.

Description

Technical field [0001] The invention relates to a production process and process of ultrapure water, in particular to an integrated membrane process production process and process of electronic grade ultrapure water. Background technique [0002] The ultrapure water referred to in the present invention refers to the removal of various suspended impurities, inorganic ions and non-ionized impurities, including various organic matter, bacteria, viruses and other microorganisms, and fine particles in the water to the limit that can be reached. "Deionized water" or "high resistivity water" or "ultra-high purity water". [0003] The national standard GB / T11446.1-1997 defines "electronic grade water" as "high-purity water used in the process of manufacturing electronic components". The highest level of electronic grade water is the cleaning water used in the production of very large scale and very large scale integrated circuits. The quality requirements of the electronics industry for ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F9/08
Inventor 王建友王世昌任延王宇新王志
Owner TIANJIN UNIV
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