Process for treating residual ammonia water of coking

A technology of ammonia water and processing technology, which is applied in the field of ammonia distillation, can solve the problems of equipment corrosion environment, large steam consumption, and many impurities in ammonia water, and achieve the effects of high product quality, good economic benefits, and reduced environmental pollution

Inactive Publication Date: 2005-06-29
JIGANG GRP
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Problems solved by technology

The remaining ammonia water is highly corrosive in the ammonia distillation process. The traditional ammonia distillation process consumes a lot of steam (200kg of steam per ton of rich liquid), and the product ammonia water has many impurities. Therefore, the coking ammonia distillation process is backward in technology and low in efficiency , high energy consumption, equipment corrosion and environmental pollution have become urgent problems to be solved

Method used

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  • Process for treating residual ammonia water of coking
  • Process for treating residual ammonia water of coking

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Embodiment Construction

[0013] In the process design of the system, the PRO-II software of SIMSCI Company of the United States is used for system simulation and optimization, and the process conditions are determined, including the organizational form of the process, the theoretical plate number and feed position of the rectification column, the temperature, pressure and concentration distribution in the column, The reflux ratio and output, heat exchanger, reboiler and condenser load, etc. are simulated and calculated by using PRO-II software for different process methods, and the traditional simple distillation process is reformed to make the ammonia distillation process a strict process. The advanced chemical distillation unit achieves strict material balance and heat balance. In the implementation of the equipment, inclined-hole trays were used as internal components, and heat transfer oil was used as the heating medium of the reboiler. Some improvements were also made in equipment materials, so th...

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Abstract

The invention has supplied a processing technique for remained ammonia water, the remained ammonia water enters into ammonia still after heat exchange in heat exchanger, the ammonia gas enters into the condenser on the top of the tower to be cooled and flows back, its characteristics are: use the world-famous software package to do simulating optimal design, the ammonia still has multi-channel compound plate with declined holes, the hot waste water at the bottom enters into the reboiling device, the steam comes back from which to the ammonia still after being heated by heat conducting oil, for supplying heat to ammonia. The invention has advanced the conventional technique direct steam distillation technology for processing remained has stable operation, remarkable effect of energy-saving, decreasing the cost, increasing the products quality as well as the economic income, more importantly, the environmental pollution is reduced greatly by eliminating the direct steam and reducing the quantity of waste water generated.

Description

Technical field [0001] The invention relates to an ammonia distillation technology for concentrating and purifying ammonia water with a relatively low ammonia content, in particular to a method for treating residual ammonia water produced in the coking industry. Background technique [0002] In the production process of the coking industry, some residual ammonia water with low ammonia content (generally 0.3-1.0%) will be produced. The residual ammonia water is the usual name for the water brought in by coking coal and coking chemical combination water in tar sewage, referred to as rich liquid. Generally, the ammonia water is treated by the distillation principle, that is, the ammonia distillation process is used to purify and concentrate it to obtain purified wastewater and product concentrated ammonia water. The remaining ammonia water is highly corrosive in the ammonia distillation process. The traditional ammonia distillation process consumes a lot of steam (200kg of stea...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C02F1/04C02F1/40C02F1/58
Inventor 汤志刚朱玉廷陈奕铨康春清卢元俭陈昌华徐文胜李维忠李德谨孟繁刚
Owner JIGANG GRP
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