Method of extracting jianiol from tobacco
A technology of solanesol and tobacco, which is applied in the field of natural product chemistry, can solve the problems of large consumption of extraction solvents, high cost of solvent use, and potential fire safety hazards, and achieve saving in operating procedures, saving of solvent usage, and fire safety The effect of low risk
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Embodiment 1
[0023] 100kg water content 16.5% offal smoke powder 80% ethanol 680kg, reflux extraction at 85°C for 2h, add NaOH 10kg after solid-liquid separation, No. 6 solvent oil 380kg, saponify at 82°C, extract for 2.5h, separate the oil phase, add water to the oil phase After washing 27 kg, wash with 5 kg of 80% ethanol, and recover the solvent from the oil phase after washing to obtain 2 kg of liquid viscous substance with a content of solanesol of 25.6%.
Embodiment 2
[0025] Add 600kg of 85% ethanol to 100kg moldy cut tobacco with water content of 14.2%, reflux and extract at 85°C for 1.5h, add KOH 6kg after solid-liquid separation, 300kg of No. 6 solvent oil, saponify and extract at 82°C for 2h, separate the oil phase, add water to the oil phase After washing 30 kg, wash with 5 kg of 80% ethanol, and recover the solvent from the oil phase after washing to obtain 2.5 kg of liquid viscous substance with a content of solanesol of 23.5%.
Embodiment 3
[0027] Add 400kg of methanol to homogenize 200kg of remaining tobacco leaves with a water content of 50.6%, then add 600kg of methanol, reflux at 65°C for 1.5h, add 12kg of NaOH after solid-liquid separation, 500kg of No. 6 solvent oil, saponify and extract at 65°C for 2h, separate The oil phase was washed with 35 kg of water and then washed with 5 kg of 80% ethanol. The solvent was recovered from the oil phase after washing to obtain 3 kg of liquid viscous substance with a content of solanesol of 26.5%.
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