Fracture end protective agent used for brittle fiber mechanics measurement, its proparation and use

A brittle fiber and protective agent technology, which is applied in the field of fracture end protective agent for mechanical measurement of brittle fibers, can solve the problems of inability to carry out tensile section analysis of brittle fibers, lack of data support for quantitative values, and fiber fracture end damage. Experimental results, convenient preparation, and the effect of improving the retention rate

Inactive Publication Date: 2006-06-28
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Existing carbon fiber tensile research (Yao Jiangwei, Yu Weidong. Influencing factors of carbon fiber monofilament tensile test, Journal of Materials Science and Engineering, 2005, 23(5): 1-4) has proved that brittle fiber tensile fracture Due to the instantaneous release of elastic potential energy, the two broken ends of the fibers will rebound at a high speed from the fracture to the direction of the clamping point, which will eventually cause the broken ends of the fibers to be damaged during the high-speed recovery and cannot be completely retained, resulting in brittle fibers. Situations where tensile section analysis cannot be performed
The protection method that this produces also has report (S.C.Bennett.D.J.Johnson.Strength-structure relationships in PAN-based carbonfibers.Journal of materials science, 1983,18:3337-3347; B.J.Jnice, B.B.John, S.Roberte.Analysis of flaws in high-strength carbon fibers from mesophase pitch.Journal of materials science, 1980, 15: 2455-2465), but whether there is indeed a retention effect and the quantitative value of the retention rate produced by the protective agent lacks data support, and there is no patent report

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Ingredients Weight% (weight percent)

[0023] White mineral oil 23.5%

[0024] Soybean Oil 14%

[0025] Glycerin 5%

[0026] water 55%

[0027] Polyglyceryl-2 Dipolyhydroxystearate 2%

[0028] Methylparaben 0.2%

[0029] Tocopherol 0.3%

[0030] In order to detect the effect of protective agent on the retention rate of fiber section, a group of comparative experiments were carried out. The experimental results prove that due to the rapid rebound of the fiber at the moment of breaking, the unprotected brittle fiber can hardly retain the real tensile section of the fiber when stretched, but the retention of the fiber tensile section is significantly improved after coating the protective agent. The detection methods of the following examples are the same.

[0031] Experimental conditions

Embodiment 2

[0033] Ingredients Weight% (weight percent)

[0034] White mineral oil 20%

[0035] Peanut Oil 9.3%

[0036] Sorbitol (70% solution) 9.5%

[0037] water 60%

[0038] Polyethylene glycol-2 sesquistearate 1%

[0039] Propylparaben 0.1%

[0040] tert-butyl hydroxytoluene 0.1%

[0041] Experimental conditions

Embodiment 3

[0043] Ingredients Weight% (weight percent)

[0044] White mineral oil 25%

[0045] Malt Oil 14%

[0046] Glycerin 5%

[0047] water 55%

[0048] Polyoxyethylene ether phosphate triester 0.8%

[0049] Phenoxyethanol 0.1%

[0050] Tocopherol 0.1%

[0051] Experimental conditions

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PUM

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Abstract

A method for preparing protectant of brittle fiber breaking end in mechanical test includes using white oil, water, wetting agent and emulsifier as main composition then carrying out water phase preparation, oil phase preparation and two phase mixed emulsification on water ¿C in- oil latex for obtaining protectant of breaking end.

Description

Technical field: [0001] The invention is a technology for intact retention of fiber fracture ends when measuring brittle fiber mechanics, and furthermore relates to a fracture end protecting agent, preparation and application for brittle fiber mechanics measurements. Background technique: [0002] The mechanical measurement of flexible fibers, including stretching, bending, shearing, and torsion, its damage is not easy to happen first, because the deformation loses energy; second, even if it is broken, its broken end can be preserved intact, which is convenient for people to understand or recognize its Fracture mechanism. Therefore, there is no problem of retention of broken ends at all. However, brittle fibers, such as carbon fibers, glass fibers, ceramic fibers, and mineral fibers, will not only fracture under small deformations when stretched, bent, sheared, and twisted, but also cause secondary fractures due to shock vibrations. , especially in conventional tensile exp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N3/00C09D191/00
Inventor 于伟东姚江薇
Owner DONGHUA UNIV
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