Chemical and machinery pulping process using complete white mulberry branch as raw material

A chemical-mechanical, mulberry branch technology, applied in the directions of pulping with inorganic alkali, pulping with organic solvents, fiber raw materials, etc., can solve the problems of long soaking time, easy accumulation, low pulp yield and strength, etc. The effect of improving the qualified rate of slices, increasing the specific surface area and making full use of resources

Inactive Publication Date: 2006-09-27
宜宾纸业股份有限公司
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Problems solved by technology

Many years ago, it was recorded in our country that the bast bark of mulberry branches was used to produce rice paper, and the production of natural color wrapping paper with the core rods of mulberry branches has been the result of our country's research in recent years. However, there is no report of using mulberry branches to mix pulp
[0004] China Patent Office discloses a kind of " mulberry bar, tobacco rod cold alkali method pulping and papermaking process " with publication number CN107092A. Pulping and papermaking. This method can be used to manufacture cigarette paper, imitation rice paper, high-grade sacrificial paper, oil-proof and waterproof base paper (food packaging paper), etc. This process is a typical chemical pulping process, specifically a cold alkali From the perspective of its technical content, although the phloem and core rod of mulberry branches are sliced ​​and mixed for pulping, there is no technical hint for making high-grade paper such as newsprint. The reason is that mulberry strips Cold soda pulping only adopts a large amount of lignin removal pulping method, without bleaching and high-consistency refining process, and the whiteness and fiber characteristics cannot meet the requirements of high-grade paper.
[0011] (1) Due to the large difference in the chemical composition of the phloem and core rods of mulberry branches, it is difficult to achieve sufficient alkalization of the phloem and core rods at the same time during the mixing pulping process, especially during the dipping process, and it is not easy to find a suitable one. Impregnation liquid and impregnation process conditions can easily lead to insufficient fiber swelling and affect the pulping effect;
[0012] (2) Since the fiber morphology of the phloem and core rods of mulberry branches is also very different, the length of the fibers varies greatly. In the process of mixing and pulping, if the fibers are too long, it is easy to accumulate during papermaking. If the fibers are too short, the quality of the paper produced The strength is not enough. Therefore, in the pulping process, it must be solved that the pulp produced meets the requirements of producing high-grade paper, but it has not been solved so far;
[0013] Just because of the above-mentioned difficulties, using mulberry branches as pulping raw materials, the prior art can only separate bast and core rods for pulping respectively, but the separation process of bast and core rods is difficult, and it is generally required to fully remove the mulberry branches before separation. Soaking, and the soaking time must be long, the water content of mulberry branches should be high, and manual separation is adopted, which cannot meet the needs of industrialized large-scale production at all. Therefore, the method of making pulp separately with bast and core rods is generally limited to manual workshops. Bast chemical pulping has a long history of making high-grade paper, such as rice paper, mirror paper, filter paper, etc. Due to the limitation of raw materials and pulping requirements, the production scale is very small. If only phloem is used as pulping raw material, due to its The proportion of mulberry branches is small. If all the bast is used for pulping and papermaking, the loss of other parts will be large and the cost will be high. How to make full use of the core rod to make high-grade paper has become an urgent and unsolved technical problem;
[0014] Second, the dust on the surface of the phloem is difficult to remove:
But this kind of pulping process has the disadvantages of low pulp yield and high production cost, and cannot be used for large-scale production requirements, and the economy is poor
[0016] The chemical pulping method is used for the whole rod, because there is no dust problem in the core rod, if the same chemical liquid is used, it will appear: or the fiber of the core rod is seriously damaged due to excessive chemical liquid, and the yield and strength of the pulp are too low; or Insufficient amount of liquid causes dust to be unable to be eradicated, there are many bast fiber bundles, and the quality of pulp is very poor, so it is difficult to accurately control the amount of liquid medicine

Method used

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  • Chemical and machinery pulping process using complete white mulberry branch as raw material

Examples

Experimental program
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Effect test

Embodiment 1

[0038] Embodiment 1: a kind of pulping process using mulberry branch as the chemical mechanical pulp of raw material, carries out as follows:

[0039] (1) slice: mulberry branch is cut into the straight section that length is 10mm;

[0040] (2) Steaming before washing: the above-mentioned straight slices are sent into the steaming chamber, and a sodium hydroxide solution (concentration of 100g / l) of 2% of the straight slice weight (net weight) is added in the steaming chamber. Under the condition of temperature of 60°C, the steaming time is 20 minutes;

[0041] (3) Washing: Wash the steamed straight slices in water at 70°C;

[0042] (4) Steaming after washing: Send the straight slices after washing into the steaming chamber, and steam for about 20 minutes under the condition that the steaming exhaust temperature is 70°C;

[0043] (5) One-stage pressing: Send the steamed straight slices into the first stage of the screw extruder to squeeze, grind and tear them under a pressur...

Embodiment 2

[0048] Embodiment 2: a kind of pulping process using mulberry sticks as raw material chemical mechanical pulp, carried out as follows:

[0049] (1) slice: mulberry branch is cut into the straight section that length is 18mm;

[0050] (2) Steaming before washing: the above-mentioned straight slices are sent into the steaming chamber, and a sodium hydroxide solution (concentration of 50g / l) of 3% of the straight slice weight (net weight) is added in the steaming chamber. The steaming time is 40 minutes at a temperature of 40°C;

[0051] (3) Washing: Wash the steamed straight slices in water at 40°C;

[0052] (4) Steaming after washing: Send the straight slices after washing into the steaming chamber, and steam for about 30 minutes under the condition that the steaming exhaust temperature is 35°C;

[0053] (5) One-stage pressing: the steamed straight slices are sent into the first stage of the screw extruder to be crushed and torn under a pressure of 1.9 kg to form compressed m...

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Abstract

This invention discloses a pulping process with mulberry bough as raw material, which comprises the following steps: slicing, steaming before scouring, scouring, steaming after scouring, first squeeze, second squeeze, steeping, reaction, post-treatment, and these steps are sequential. The invention improves percent of pass of slicing mulberry bough and availability ratio of pulp in the core, and has good dust collection efficiency. With mixing pulping of mulberry bough, the bore rod with short fibre and large content can be used fully, and the finished pulp can be used in top grade paper. With fully using resource is, the process settles said technical matters, and it is suit for use in commercial manufacture.

Description

technical field [0001] The invention relates to a papermaking pulping process, in particular to a chemical mechanical pulping process using mulberry branches as raw materials. Background technique [0002] With the technological progress of the paper industry and the increase of paper consumption, the raw material structure of papermaking is also constantly evolving. As one of China's "Four Great Inventions", papermaking was born in the Cai Lun era in the Eastern Han Dynasty. At that time, the raw materials for papermaking were rags and fishing nets mainly made of hemp; in the Tang and Song Dynasties, hemp, bark, and straw were used for papermaking. and other raw materials; then people found that wood is better than other raw materials because of its fiber shape, and it is easy to produce various high-quality products, with high production efficiency, easy pollution control, dense volume, easy transportation and storage, and is more suitable than other raw...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C3/02D21C3/04D21C3/20D21B1/04D21B1/12D21B1/34D21C1/02D21C1/06D21C1/08D21D1/20
Inventor 明治凯梁家强缪友权王希木伍元俊周键
Owner 宜宾纸业股份有限公司
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