Technological process of producing fire retardant antiflux fiber
A process method and anti-melting technology, applied in the direction of fiber chemical characteristics, fire-proof and flame-retardant filament manufacturing, single-component cellulose artificial filament, etc., can solve the problem that the quality of flame retardants cannot meet the spinning requirements, and the handle feels astringent , poor alkali resistance and other problems
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Embodiment 1
[0018] Example 1: 1.67dtex*38mm flame-retardant and anti-melt fiber
[0019] Using cellulose pulp as raw material, through the known steps of dipping, pressing, pulverizing and aging, 36Kg of alkali cellulose is obtained, and the content of methyl cellulose or alpha cellulose in the alkali cellulose is 30%.
[0020] 20KgSiO Content is 21% sodium silicate nonahydrate (Na 2 SiO 3 9H 2 O) join in 60L yellowing dissolving water and make solution, join this solution in the alkali cellulose in 36Kg yellowing, make it fully dissolve, mix through stirring, make total solid content be 11.5% (mass), sodium hydroxide Viscose with a content of 7.24% is filtered and matured to obtain spinning glue, which is spun in a coagulation acid bath with a sulfuric acid content of 110g / l, sodium sulfate 330g / l, zinc sulfate 10g / l, and a temperature of 48°C. Stretching produces 1.67dtex*38mm short fibers. After the fibers are acid-washed and washed neutral, they are cross-linked in a cross-linking...
Embodiment 2
[0022] Example 2: 3.33dtex*60mm flame-retardant and anti-melt fiber
[0023] Using cellulose pulp as raw material, through known steps of soaking, pressing, pulverizing and aging, 36Kg of alkali cellulose is obtained, and the content of methyl cellulose or alpha cellulose in the alkali cellulose is 30%.
[0024] 10KgSiO 2 Potassium silicate (K 2 SiO 3 ) was added to 30L yellowing dissolved water to make a solution, the solution was added to the alkali cellulose in 36Kg yellowing, and it was fully dissolved and mixed by stirring to obtain a total solid content of 9.35% (mass), and the sodium hydroxide content 6.26% viscose, filtered and matured to obtain spinning glue, spun in a coagulation acid bath with a sulfuric acid content of 85g / l, sodium sulfate 320g / l, zinc sulfate 15g / l, and a temperature of 40°C. 3.33dtex*60mm short fibers are produced. After the fiber is neutralized by water washing, it is cross-linked in a potassium metaaluminate cross-linking bath with a conce...
Embodiment 3
[0026] Example 3: 2.78dtex*51mm flame-retardant and anti-melt fiber
[0027] Using cellulose pulp as raw material, through known steps of soaking, pressing, pulverizing and aging, 36Kg of alkali cellulose is obtained, and the content of methyl cellulose or alpha cellulose in the alkali cellulose is 30%.
[0028] 30KgSiO Content is 21% sodium silicate nonahydrate (Na 2 SiO 3 9H 2 O) this solution is added into 70L yellowing dissolving water to make solution, joins in the alkali cellulose in 36Kg yellowing, makes total solid content and is 8.20% (mass), the viscose of sodium hydroxide content 5.24%, after filtering , matured to obtain spinning glue, spun in a coagulation acid bath with a sulfuric acid content of 120g / l, sodium sulfate 330g / l, aluminum sulfate 6g / l, and a temperature of 48°C, and produced short fibers of 2.78dtex*51mm after proper drafting . After the fiber is neutralized by water washing, it is cross-linked in a sodium metaaluminate cross-linking bath with a...
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