Sn-Cu-Cr lead-free soldering material and its preparation
A lead-free solder, sn-cu-cr technology, applied in welding equipment, welding/cutting medium/material, welding medium, etc., can solve unsatisfactory anti-oxidation and corrosion performance, cost increase, alloy melting point, welding reliability , process yield and insufficient oxidation resistance
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Embodiment 1
[0023] The preparation of embodiment 1 Sn-Cu0.7-Cr0.3:
[0024] According to the weight percentage, Cu is 0.7% and Cr is 0.3%. Prepare 5.0kg of Sn-Cu10 master alloy and 5.0kg of Sn-Cr7.5 master alloy in a vacuum medium-frequency induction melting furnace. During the preparation process: ① first melt the weighed pure Sn in a vacuum induction melting furnace to 650°C, Add the weighed pure Cu flakes, stir and melt until the furnace temperature is 500-600°C, stir and keep warm for 10 minutes, pour into a square ingot to prepare a Sn-Cu10 master alloy; ②First put the weighed pure Sn in a vacuum medium frequency induction furnace Melt, add the weighed pure Cr block, stir and melt until the furnace temperature is 1300-1400°C, stir and keep warm for half an hour, pour into a square ingot to prepare a Sn-Cr7.5 alloy; analyze the uniformity of each master alloy composition. Take 14.0g of Sn-Cu10 master alloy, 8.00g of Sn-Cr7.5 master alloy, and 178.0g of pure Sn. Then melt pure Sn in ...
Embodiment 2
[0025] The preparation of embodiment 2 Sn-Cu0.2-Cr0.1:
[0026] Proportion calculated by weight percentage, Cu is 0.2%, Cr is 0.1%. The preparation of the master alloy is the same as in Example 1. Weigh 4.0g of Sn-Cu10 master alloy, 2.70g of Sn-Cr7.5 master alloy, and 193.3g of pure Sn. First melt pure Sn in a resistance furnace and heat it to 300°C, then add Sn-Cu10 master alloy and Sn-Cr7.5 master alloy in turn, heat it to 300°C and keep it for 10 minutes, pour it into a cylindrical mold, and wait until the ingot is completely solidified Then remelt the ingot to 300°C and keep it warm for 10 minutes, pull out the surface oxide slag, and pour it into a mold to make an ingot for use.
Embodiment 3
[0027] The preparation of embodiment 3 Sn-Cu0.9-Cr0.6:
[0028] Proportion calculated by weight percentage, Cu is 0.9%, Cr is 0.6%. The preparation of the master alloy is the same as in Example 1. Weigh 18.0g of Sn-Cu10 master alloy, 16.0g of Sn-Cr7.5 master alloy, and 166.0g of pure Sn. First melt pure Sn in a resistance furnace and heat it to 300°C, then add Sn-Cu10 master alloy and Sn-Cr7.5 master alloy in turn, heat it to 300°C and keep it for 10 minutes, pour it into a cylindrical mold, and wait until the ingot is completely solidified Then remelt the ingot to 300°C and keep it warm for 10 minutes, pull out the surface oxide slag, and pour it into a mold to make an ingot for use.
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