Grease, rolling bearing, constant velocity joint and rolling parts
A technology for rolling bearings and rotating parts, applied in the field of lubricating grease, can solve problems such as lubricating oil film rupture, and achieve the effect of preventing wear
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Embodiment 1~ Embodiment 11
[0163] In the reaction vessel, add a thickener to the base oil and homogenize it with a three-roll mill to obtain the lithium soap / mineral oil-based grease shown in Table 1 (40°C base oil viscosity 100mm 2 / s, mixed consistency 220), urea / PAO oil grease (base oil viscosity 46mm at 40°C 2 / s, mixed consistency 280), lithium soap / ester oil-based grease (base oil viscosity 33mm at 40°C 2 / s, mixed consistency 250), urea / ether oil-based grease (40°C base oil viscosity 100mm 2 / s, mixing consistency 300).
[0164] Furthermore, bismuth or inorganic bismuth was used as an extreme pressure agent, and was added to the above-mentioned grease at the ratio shown in Table 1 to prepare the grease of each example. The obtained grease was subjected to the following extreme pressure resistance evaluation test and rolling bearing test, and the results are shown in Table 1.
Embodiment 12
[0189] Immerse a steel plate (SUJ2 thickness 10mm) and a φ40mm× For a ring test piece (SUJ2) with a thickness of 10 mm, the end surface of the ring test piece was pressed against the steel plate with a load of 490 N, and the ring test piece was rotated at 2000 rpm for 20 hours. The bismuth trioxide film was formed on the end surface of the ring test piece due to frictional heat at this time and the like. Surface analysis by photoelectric spectroscopy (hereinafter abbreviated as XPS) confirmed that a coating of bismuth trioxide was formed on the end face of the ring-shaped test piece.
[0190] Using two of these ring-shaped test pieces, the following extreme pressure resistance evaluation test was implemented. show the result in Figure 14 .
Embodiment 13
[0192] Dip a steel plate (SUJ2 thickness 10mm) and φ40mm×thickness 10mm in a liquid with a ratio of 95g of PAO oil (Silver 801, manufactured by Nippon Steel Chemical Co., Ltd.) and 5g of bismuth (manufactured by Wako Pure Chemical Industries, Ltd.). For the ring test piece (SUJ2), the end face of the ring test piece was pressed against the steel plate with a load of 490N, and the ring test piece was rotated at 2000 rpm for 20 hours. Due to the frictional heat at this time, a bismuth coating was formed on the end surface of the ring test piece.
[0193] Surface analysis by XPS confirmed that a bismuth coating was formed on the end surface of the ring test piece.
[0194] As two of the ring test pieces, the following extreme pressure resistance evaluation test was implemented. show the result in Figure 14 .
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