A non-crystal sold film material Ag1-x-yGexSey and making method and its application
A thin-film material and amorphous technology, applied in metal material coating technology, static memory, ion implantation plating, etc., can solve the problems of complex structure, low access speed, large volume, etc., and achieve simple and simplified component structure The effect of production process and small device size
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[0060] Embodiment 1. The preparation method of solid electrolyte amorphous AGS thin film material used to prepare non-volatile phase change memory element, the preparation steps are as follows:
[0061] (1) AGS alloy target (9) is made by suspension smelting cold crucible equipment: the ratio of Ag, Ge, Se mixture is 33% mol Ag, 20% molGe and 47% molSe, and the ratio is good when melting at 600℃. The mixture of Ge and Ge forms an alloy, and then the silver-germanium alloy and Se are continuously smelted at 500° C. to form a block, and the obtained block is polished and cut into a circular target.
[0062] (2) Fix the AGS target (9) on the target stage (10) of the pulsed laser deposition film forming system, the substrate (6) on the substrate stage (13), and the resistance heating furnace (15) on the substrate Below the stage (13), they are all placed in the growth chamber (11) of the pulsed laser deposition film-making system;
[0063] (3) Vacuum the growth chamber (11) to 5×10 th...
Example Embodiment
[0067] Embodiment 2. The preparation method of the non-volatile phase change memory device based on the solid electrolyte amorphous AGS film, the preparation steps are as follows:
[0068] (1) The non-reactive electrode film 2 is deposited on the silicon wafer substrate 1 by a pulsed laser deposition method, the material of which is platinum, and the thickness of the non-reactive electrode film 2 is 200 nanometers;
[0069] (2) A layer of insulating layer 3 is deposited on the non-reactive electrode film 2 by means of radio frequency magnetron sputtering, the material of the insulating layer is silicon dioxide, and its thickness is 100 nanometers;
[0070] (3) Using focused particle beam etching in the insulating layer 2 to process micro holes with a diameter of 100 nanometers, exposing the lower non-reactive electrode film 2;
[0071] (4) Cover the substrate on which the micro-holes 5 are processed with a metal mask engraved with a hole with a diameter of 0.5 mm, and the holes of...
Example Embodiment
[0076] Embodiment 3. The preparation method of the non-volatile phase change memory device based on the solid electrolyte amorphous AGS film, the specific preparation steps are as follows:
[0077] (1) A layer of insulating layer 2 is deposited on the high-conductivity silicon substrate 2 by radio frequency magnetron sputtering. The material of the insulating layer is silicon dioxide with a thickness of 200 nanometers. A silicon dioxide ceramic target is used during sputtering. , Use argon gas with a pressure of 10 Pa as the sputtering gas, and the low temperature of the lining is 80 ℃;
[0078] (2) Using focused ion beam etching to process micro-holes with a diameter of 1 micron in the insulating layer 3, exposing the lower high-conductivity silicon non-reactive electrode 2;
[0079] (3) Cover the substrate on which the micro-holes are processed with a metal mask engraved with holes with a diameter of 0.4 mm, and the holes of the mask are aligned with the micro-holes 5;
[0080] ...
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