NiAl-Cr(Mo) biphase eutectic crystal intermetallic compound modified by Ta
A technology of intermetallic compounds and eutectic metals, which is applied in the field of Ta-modified NiAl-Cr(Mo) double-phase eutectic intermetallic compounds, which can solve the problems of little improvement in high temperature strength and failure to meet the use requirements.
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Embodiment 1
[0030] Example 1: Preparation of 33Ni-28Al-30Cr-4Mo-5Ta intermetallic compound
[0031] The ingredients are formulated according to the composition of 33Ni-28Al-30Cr-4Mo-5Ta (atomic percentage), and the purity of the raw materials is 99.999%.
[0032] Melting 33Ni-28Al-30Cr-4Mo-5Ta alloy ingots in a non-consumable vacuum electric arc furnace with a vacuum degree of 5×10 -3 Pa, smelting temperature 3000°C, smelting 4 times, the raw materials are smelted evenly.
[0033] The obtained intermetallic compound rod was kept at 1200° C. for 12 hours in a high-temperature heat treatment furnace, and then cooled to room temperature with the furnace.
[0034] A cylindrical sample with a diameter of 6mm and a height of 9mm and a square cylinder with a diameter of 6mm×6mm×30mm were cut from the heat-treated 33Ni-28Al-30Cr-4Mo-5Ta ingot by the wire cutting method for mechanical performance testing.
[0035] Accurate to 10 with Model 1111 -4 The mass M of the sample is measured by an ele...
Embodiment 2
[0037] Example 2: Preparation of 33Ni-30Al-30Cr-4Mo-3Ta intermetallic compound
[0038] The ingredients are 33Ni-30Al-30Cr-4Mo-3Ta (atomic percentage), and the purity of the raw materials is 99.999%.
[0039] Melting 33Ni-30Al-30Cr-4Mo-3Ta alloy ingots in a non-consumable vacuum electric arc furnace with a vacuum degree of 3×10 -3 Pa, the melting temperature is 2700°C, smelting 6 times, and the raw materials are smelted evenly.
[0040] The obtained intermetallic compound rod was kept at 1200° C. for 12 hours in a high-temperature heat treatment furnace, and then cooled to room temperature with the furnace.
[0041] The mechanical property test condition of 33Ni-30Al-30Cr-4Mo-3Ta intermetallic compound is identical with embodiment 1, and its density is 6.28g / cm 3 See Figure 2. In the figure, the yield strength at 25°C is 1380MPa, and the compression plasticity is greater than 20%; the yield strength at 800°C is 450MPa, and the compression plasticity is greater than 35%; th...
Embodiment 3
[0042] Example 3: Preparation of 33Ni-25Al-30Cr-4Mo-8Ta intermetallic compound
[0043] The ingredients are formulated according to the composition of 33Ni-25Al-30Cr-4Mo-8Ta (atomic percentage), and the purity of the raw materials is 99.999%.
[0044] Melting 33Ni-25Al-30Cr-4Mo-8Ta alloy ingots in a non-consumable vacuum electric arc furnace with a vacuum degree of 4×10 -3 Pa, smelting temperature 3000°C, smelting 4 times, the raw materials are smelted evenly.
[0045] The obtained intermetallic compound rod was kept at 1200° C. for 12 hours in a high-temperature heat treatment furnace, and then cooled to room temperature with the furnace.
[0046] The mechanical property test condition of 33Ni-25Al-30Cr-4Mo-8Ta intermetallic compound is identical with embodiment 1, and its density is 6.51g / cm 3 See Figure 3. In the figure, the yield strength at 25°C is 1880MPa, and the compression plasticity is greater than 15%; the yield strength at 800°C is 720MPa, and the compression p...
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