Nano combination electrode material Li3N/Si used for lithium ion battery and its preparation method
A lithium-ion battery and nano-composite technology, which is applied in battery electrodes, electrode manufacturing, metal material coating processes, etc. The effect of improving the utilization rate and simple preparation process
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[0010] Li with a molar ratio of 1:1 3 N and Si powder are fully mixed; then the mixture powder is pressed into a target material for pulse laser deposition, and a composite nano-mixture electrode film material is prepared by a pulse laser deposition method. Preparation conditions: the substrate is a stainless steel sheet, the distance between the substrate and the target is 30 mm; the deposition process is carried out in high-purity nitrogen, and the pressure is kept at 10 Pa; the deposition temperature is room temperature; the laser wavelength is 355 nm, the pulse frequency is 10 Hz, and the pulse width is 10 ns. The energy density is 2J / cm 2 ; The deposition time was 1 hour.
[0011] It was shown by SEM that the particle size in the deposited film was about 50nm. Indicating that the deposited film is Li 3 N / Si nanocomposite material. It was determined by TEM electron diffraction that the deposited film was Li 3 N / Si nano-hybrid, where Li 3 N is a hexagonal structure, a...
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