Light-blocking resin composition, color filter, and liquid crystal display
A resin composition, light-shielding technology, applied in the directions of optics, filters, optical elements, etc., can solve the problem of inability to achieve developability, resolution, adhesion, developability, resolution, adhesion, linearity, Insufficient improvement of adhesion, etc.
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[0280] The present invention will be further described in detail by citing synthesis examples, examples and comparative examples below, but as long as it does not exceed the scope of the present invention, the present invention is not limited to the description of the following examples.
Synthetic example -1
[0282] Synthesis example-1 (preparation of polymer dispersant solution)
[0283] 32 g of a trimer of toluene diisocyanate (manufactured by Mitsubishi Chemical Corporation "Maitec GP750A", resin solid content of 50% by weight, butyl acetate solution) and 0.02 g of dibutyltin dilaurate as a catalyst were mixed with 47 g of propylene glycol monomethyl ether ether. acid ester (PGMEA) for dilution and dissolution. 14.4 g of polyethylene glycol having a methoxy group at one end and a number average molecular weight of 1,000 (manufactured by NOF Co., Ltd. "Unioux M-1000") and 9.6 g of polypropylene glycol with a number average molecular weight of 1,000 ( A mixture of "Sannex PP-1000" manufactured by Sanyo Chemical Industry Co., Ltd.) was further reacted at 70° C. for 3 hours. Next, 1 g of N,N-dimethylamino-1,3-propanediamine was added, and the mixture was further reacted at 40° C. for 1 hour. The amine value of the solution containing the polymer dispersant thus obtained was determ...
Synthetic example -2
[0284] Synthesis Example-2 (Synthesis of Binder Resin)
[0285]Add 300 parts by weight of "XD1000" manufactured by Nippon Kayaku Co., Ltd. (polyglycidyl ether of dicyclopentadiene-phenol polymer, weight average molecular weight is 700, epoxy equivalent is 252), 87 parts by weight of acrylic acid , 0.2 parts by weight of p-methoxyphenol, 5 parts by weight of triphenylphosphine, and 255 parts by weight of PGMEA were stirred at 100° C. until the acid value was 3.0 mg-KOH / g. It took 9 hours to reach the target acid value (acid value 2.5 mg-KOH / g). Next, 145 parts by weight of tetrahydrophthalic anhydride was further added and reacted at 120° C. for 4 hours to obtain a binder resin I having an acid value of 100 mg-KOH / g and a weight average molecular weight of 2600 in terms of polystyrene as measured by GPC. solution.
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