Method for preparing lithium battery anode
A lithium battery and positive electrode technology, applied in the field of preparation of lithium battery positive electrodes, can solve the problems of reduced electrode specific capacity, complex process, high cost, etc., and achieve the effect of increased specific capacity, simple manufacturing process, and low cost
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Embodiment 1
[0022] The aluminum foil with a flat surface is cut into a disc with a diameter of 12 mm, first ultrasonically washed with acetone for 3 minutes, then ultrasonically washed with distilled water for 1 minute, taken out and dried.
[0023] Put the processed aluminum foil into the vacuum chamber of the RF chemical vapor deposition device, use Ar to carry the thiophene into the reaction vacuum chamber, adjust the gas flow to maintain the pressure in the chamber at 2.5 Pa, and adjust the RF power source to 100W. The total flow of Ar and thiophene is 100 sccm (standard condition ml / min), and the volume content of thiophene is 70%. After 5 hours of deposition, a sulfur-carbon composite material is obtained. After it is naturally cooled to room temperature in a vacuum chamber, a lithium battery cathode is obtained .
Embodiment 2
[0025] The copper foil with a flat surface is cut into a disc with a diameter of 15 mm, first ultrasonically washed with acetone for 3 minutes, then ultrasonically washed with distilled water for 1 minute, and then taken out and dried.
[0026] Put the processed copper foil into the vacuum chamber of the radio frequency chemical vapor deposition device, and use N 2 CS 2 Carry to the reaction chamber, adjust the gas flow rate to maintain the pressure in the chamber at 6Pa, adjust the RF power source to 70W, N 2 And CS 2 The total flow is 150sccm, where CS 2 Its volume content is 60%. After 6 hours of deposition, a sulfur-carbon composite material is obtained. After it is naturally cooled to room temperature in a vacuum chamber, a lithium battery positive electrode is obtained.
Embodiment 3
[0028] The nickel foil with a flat surface is cut into a disc with a diameter of 14 mm, first ultrasonically washed with acetone for 3 minutes, then ultrasonically washed with distilled water for 1 minute, and then taken out and dried.
[0029] Put the processed nickel foil into the vacuum chamber of the hot-wire chemical vapor deposition device, adjust the wire base distance to 14mm, and use Ar to remove the CS 2 Carry to the reaction chamber, adjust the heating wire power to keep the heating wire temperature at 1600℃, adjust the needle valve to keep the growth pressure at 200Pa, Ar and CS 2 The total flow is 200sccm, where CS 2Its volume content is 65%. The sulfur-carbon composite material is obtained after 4 hours of deposition, and the anode of the lithium battery is obtained after it is naturally cooled to room temperature in a vacuum chamber.
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