Extraction technique of burdock, soja or garlic extract
A garlic extract and soybean technology, which is applied in the molding or processing of animal feed, animal feed, food science, etc., can solve the problems of affecting extraction efficiency, complex main component process, uneven extraction efficiency, etc., and achieve simple and effective operation. , the effect of reliable extraction process, high promotion and application value
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Embodiment 1
[0030] Embodiment 1: the burdock root is cut into slices, air-dried or oven-dried, crushed, added water, placed on a constant temperature water bath shaker for extraction, a total of 3 extractions, the extraction conditions are: material-water-solid-liquid ratio 1:20 (weight ratio) , extraction time 1h, extraction temperature 70°C.
[0031] Suction filtration was carried out after extraction, and the filtrate was collected. Concentrate the filtrate at 60°C and 0.08Mpa to 1 / 3 of the original volume. Add absolute ethanol 3 times the volume of the concentrated solution to the concentrated solution, stir well and place in the refrigerator to refrigerate overnight. The supernatant was discarded and the remainder was centrifuged. The resulting precipitate was freeze-dried on a vacuum freeze dryer to finally obtain a powdered burdock extract.
Embodiment 2
[0032] Example 2: After crushing the soybeans, add water, place on a constant temperature water bath shaker for extraction, extract 3 times in total, the extraction conditions are as follows: material-water-solid-liquid ratio 1:10 (weight ratio), extraction time 1.5h, extraction temperature 80 ℃.
[0033] Suction filtration was carried out after extraction, and the filtrate was collected. The filtrate was concentrated at 60°C and 0.08Mpa, and the concentrated volume was reduced to 1 / 4 of the original volume. Add 95% ethanol 4 times the volume of the concentrated solution to the concentrated solution, stir well and refrigerate overnight in the refrigerator. The supernatant was discarded and the remainder was centrifuged. The resulting precipitate was freeze-dried on a vacuum freeze dryer to finally obtain a powdered soybean extract.
Embodiment 3
[0034] Example 3: After crushing the fresh garlic sample, add water, place it on a constant temperature water bath shaker for extraction, extract 3 times in total, and the extraction conditions are as follows: material-water-solid-liquid ratio 1:20 (weight ratio), extraction time 2h, extraction The temperature is 90°C.
[0035]Suction filtration was carried out after extraction, and the filtrate was collected. The filtrate was concentrated at 60°C and 0.08Mpa, and the concentrated volume was reduced to 1 / 4 of the original volume. Add 95% ethanol 3.5 times the volume of the concentrated solution to the concentrated solution, stir well and refrigerate overnight in the refrigerator. The supernatant was discarded and the remainder was centrifuged. The resulting precipitate was freeze-dried on a vacuum freeze dryer to finally obtain a powdered garlic extract.
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