Low fluorescent film forming filtrate reducer and preparation method thereof
A filtrate reducer and low fluorescence technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problem of poor resistance to high temperature, salt resistance and cuttings pollution, failure to meet environmental protection requirements, and unfavorable well wall stability and other issues, to meet the requirements of environmental protection, to facilitate the stability of the wellbore wall, and to improve the perforation oil recovery.
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Embodiment 1
[0027] Take the preparation of 1000 kg of low-fluorescence film-forming fluid loss additive as an example: weigh each raw material according to the following weight. Cotton cake: 700 kg; paraffin wax: 296 kg; prepare 1% sodium hydroxide aqueous solution with sodium hydroxide and water at a ratio of 1:100, weigh 3 kg; spatula 80: 1 kg. Carry out according to the step of following preparation method:
[0028] (1), 700 kilograms of cotton cakes are pulverized to make cotton cake powder, pass through a 60-mesh sieve, and go through delinting treatment for subsequent use.
[0029] (2), put 296 kilograms of paraffin into the kneader, heat up to 90 ℃ and make it melt.
[0030] (3) After the paraffin wax is completely melted, add 700 kg of cotton cake powder for later use and stir, the temperature is maintained at 60° C., and the reaction time is 1.5 hours.
[0031] (4) After the reaction time of 1.5 hours is up, add 3 kg of 1% sodium hydroxide aqueous solution and stir evenly. The ...
Embodiment 2
[0037] Take the preparation of 1500 kg of low-fluorescence film-forming fluid loss additive as an example: weigh each raw material according to the following weight. Cotton cake: 1050 kg; paraffin wax: 444 kg; uniformly mix sodium hydroxide and water at a ratio of 1:100 to prepare a 1% aqueous solution of sodium hydroxide, weigh 4.5 kg; Span 80: 1.5 kg. Carry out according to the step of following preparation method:
[0038] (1), 1050 kilograms of cotton cakes are pulverized into cotton cake powder, passed through a 60-mesh sieve, and treated for subsequent use after delinting.
[0039] (2), 444 kilograms of paraffins are put into the kneader, be heated up to 90 ℃ and make it melt.
[0040] (3) After the paraffin wax is completely melted, add 1050 kg of cotton cake powder for later use and stir, the temperature is maintained at 60° C., and the reaction time is 1.5 hours.
[0041] (4) After the reaction time of 1.5 hours is up, add 4.5 kilograms of 1% sodium hydroxide aqueou...
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