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Low fluorescent film forming filtrate reducer and preparation method thereof

A filtrate reducer and low fluorescence technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problem of poor resistance to high temperature, salt resistance and cuttings pollution, failure to meet environmental protection requirements, and unfavorable well wall stability and other issues, to meet the requirements of environmental protection, to facilitate the stability of the wellbore wall, and to improve the perforation oil recovery.

Inactive Publication Date: 2010-12-22
湖北龙海化工有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the use of a large amount of polymer materials, the fluid loss control agents used in the prior art are not only expensive, the production process is complicated, and a large amount of substances polluting the environment are produced, but also they have poor resistance to high temperature, salt, and cuttings pollution, which is not conducive to well wall Stable, can not meet environmental protection requirements

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Take the preparation of 1000 kg of low-fluorescence film-forming fluid loss additive as an example: weigh each raw material according to the following weight. Cotton cake: 700 kg; paraffin wax: 296 kg; prepare 1% sodium hydroxide aqueous solution with sodium hydroxide and water at a ratio of 1:100, weigh 3 kg; spatula 80: 1 kg. Carry out according to the step of following preparation method:

[0028] (1), 700 kilograms of cotton cakes are pulverized to make cotton cake powder, pass through a 60-mesh sieve, and go through delinting treatment for subsequent use.

[0029] (2), put 296 kilograms of paraffin into the kneader, heat up to 90 ℃ and make it melt.

[0030] (3) After the paraffin wax is completely melted, add 700 kg of cotton cake powder for later use and stir, the temperature is maintained at 60° C., and the reaction time is 1.5 hours.

[0031] (4) After the reaction time of 1.5 hours is up, add 3 kg of 1% sodium hydroxide aqueous solution and stir evenly. The ...

Embodiment 2

[0037] Take the preparation of 1500 kg of low-fluorescence film-forming fluid loss additive as an example: weigh each raw material according to the following weight. Cotton cake: 1050 kg; paraffin wax: 444 kg; uniformly mix sodium hydroxide and water at a ratio of 1:100 to prepare a 1% aqueous solution of sodium hydroxide, weigh 4.5 kg; Span 80: 1.5 kg. Carry out according to the step of following preparation method:

[0038] (1), 1050 kilograms of cotton cakes are pulverized into cotton cake powder, passed through a 60-mesh sieve, and treated for subsequent use after delinting.

[0039] (2), 444 kilograms of paraffins are put into the kneader, be heated up to 90 ℃ and make it melt.

[0040] (3) After the paraffin wax is completely melted, add 1050 kg of cotton cake powder for later use and stir, the temperature is maintained at 60° C., and the reaction time is 1.5 hours.

[0041] (4) After the reaction time of 1.5 hours is up, add 4.5 kilograms of 1% sodium hydroxide aqueou...

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PUM

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Abstract

The invention relates to a hypofluorescence film forming filtrate reducer and a preparation method thereof, which belong to the technical field of chemical engineering additive for oil drilling. The hypofluorescence film forming filtrate reducer is prepared from cotton cake powder, olefin, 1 percent of aqueous sodium hydroxide solution and span 80. The filtrate reducer has a simple production process, low manufacturing cost, good capacity for high-temperature resistance and salt resistance, hypofluorescence, nontoxicity, small filtration loss amount and good lubricating performance, can meetthe requirement of environmental protection, effectively reduces the dynamic filtration loss amount and dynamic filtration velocity, is favorable for the stability of well wall, improves oil extraction rate of perforation, prevents a drilling fluid and a filtrate from penetrating into a mud shale body, effectively prevents stratum from hydrating, expanding and collapsing, is smooth to pull out and run into holes, prevents blocking and clamping, and solves the problems that the prior filtrate reducer uses mass macromolecular materials, has high price and a complex production process, produces mass substances polluting environment, has poor capacity for resisting high temperature, salt and drill chip contamination and is not favorable for the stability of the well wall. The hypofluorescencefilm forming filtrate reducer can be used for a straight drilling well, an inclined well and a horizontal well.

Description

Technical field: [0001] The invention relates to a low-fluorescence film-forming fluid loss reducer and a preparation method thereof, belonging to the technical field of chemical additives for petroleum drilling. Background technique: [0002] In oil drilling operations, when the drilling fluid flows through the permeable layer under pressure, it will infiltrate, causing the liquid phase of the drilling fluid to seep into the formation. This process is called "water loss". If water loss cannot be well controlled, a large amount of water loss entering the formation will not only induce wellbore instability, but also cause damage to oil and gas formations. At present, the effective way to solve this problem is to add fluid loss control agent in the drilling fluid. [0003] Fluid loss reducer is a chemical additive used in oil drilling. Its main purpose is to seal the fluid between the formations and support the casing to form a solid-free drilling mud system, reduce water los...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/44
Inventor 刘仁富
Owner 湖北龙海化工有限公司
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