Copper germinate nano-wire and preparation thereof
A copper germanate and nanowire technology, applied in chemical instruments and methods, germanium compounds, inorganic chemistry, etc., can solve problems such as no copper germanate nanowire structure, achieve batch preparation, simple preparation process, The effect of low growth temperature
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[0029]Example 1: A copper sheet with a size of about 6×2cm was ultrasonically cleaned in distilled water for ten minutes, and then fixed on the stainless steel bracket in the middle of the reactor, and then 1% of the solvent weight of germanium dioxide was mixed with distilled water Placed in a sealed reactor, the total amount of germanium dioxide and solvent accounts for 5% of the reactor vessel. Under the uniform stirring of a magnetic stirrer, the temperature is 200℃ and the pressure is 1-2MPa for 24 hours, and it is prepared on a copper sheet. The velvet-like light blue deposits uniformly deposited on the surface were obtained, and copper germanate nanowires with a length greater than 10 μm, a relatively uniform diameter distribution, and an average diameter of about 100 nm were obtained.
Example Embodiment
[0030] Example 2: A copper sheet with a size of about 6×2cm was ultrasonically cleaned in distilled water for ten minutes, and then fixed on the stainless steel bracket in the middle of the reactor, and then germanium dioxide accounting for 5% by weight of the solvent was mixed with distilled water Placed in a sealed reactor, the total amount of germanium dioxide and solvent accounts for 5% of the reactor vessel. Under the uniform stirring of a magnetic stirrer, the temperature is 200°C and the pressure is 1-2MPa for 12 hours, and it is prepared on a copper sheet. The velvet-like light blue deposits uniformly deposited on the surface were obtained, and copper germanate nanowires with a length greater than 10 μm, a relatively uniform diameter distribution, and an average diameter of about 100 nm were obtained.
Example Embodiment
[0031] Example 3. A copper sheet with a size of approximately 6×2cm was ultrasonically cleaned in distilled water for ten minutes, and then fixed on the stainless steel bracket in the middle of the reactor, and then germanium dioxide accounting for 5% of the weight of the solvent was mixed with distilled water Placed in a sealed reactor, the total amount of germanium dioxide and solvent accounted for 8% of the reactor vessel. Under the uniform stirring of a magnetic stirrer, it was kept at a temperature of 250°C and a pressure of 2-4 MPa for 24 hours, and it was prepared on a copper sheet. The velvet-like light blue deposits uniformly deposited on the surface were obtained, and copper germanate nanowires with a length greater than 10 μm, a relatively uniform diameter distribution, and an average diameter of about 100 nm were obtained.
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