Method for preparing fungal polysaccharide
A fungal polysaccharide and vacuum technology, applied in the field of preparation of fungal polysaccharides, can solve the problems of large solvent consumption, environmental pollution, low energy utilization rate, etc., and achieve the effect of saving steam consumption, shortening the extraction cycle, and remarkable energy saving effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0025] A method for preparing fungal polysaccharides, comprising the following processing steps:
[0026] (1) Raw material crushing and extractant mixing
[0027] Wash and dry the raw materials for extracting and preparing fungal polysaccharides (lotus fungi, shiitake mushrooms, and Hericium erinaceus) at low temperature (30°C), then crush them into 60-100 μm particles, and mix them with extractant water at a mass ratio of 1:3.5 Uniform;
[0028] (2) Extraction
[0029] The above-mentioned raw materials and extractant mixed solution are subjected to solvent multi-stage circulation dynamic thermal reflux extraction in a multi-functional extractor, the extraction temperature is 35 ° C, pH = 4.5, and the solvent reflux rate is 5%. Reflux) extract 40 minutes;
[0030] (3) Filtration and concentration
[0031] The above-mentioned extraction solution extracted for a certain period of time is directly vacuum-transported to an external circulation heating double-effect vacuum conc...
Embodiment 2
[0037] The same as the steps of Example 1, the difference is:
[0038] (1) Put the raw materials for extracting and preparing fungal polysaccharides (lotus fungi, shiitake mushrooms, and Hericium erinaceus) at 50°C and dry them, then crush them into 2500-3000 μm particles, and mix them with extractant water at a mass ratio of 1:8 ;
[0039] (2) The extraction conditions are: extraction temperature 100°C, pH=6.5, solvent reflux rate 15% under the conditions of reflux (using 2-stage solvent circulation dynamic heat reflux) for extraction for 70 minutes;
[0040] (3) Concentration: Concentrate for 3 hours at a vacuum of 0.05MPa and a temperature of 65°C;
[0041] (4) Alcohol precipitation: add 3 times of 95% food grade or above alcohol according to the volume ratio, stir evenly and let stand for 80 minutes;
[0042] (5) Drying: Add 8 times of distilled water or other solvents to the above-mentioned alcohol precipitates according to the mass ratio and stir to dissolve them, and ...
Embodiment 3
[0044] The same as the steps of Example 1, the difference is:
[0045] (1) Put the raw materials for extracting and preparing fungal polysaccharides (lotus fungi, shiitake mushrooms, and Hericium erinaceus) at 65°C and dry them, then crush them into particles of 6500-7000 μm, and mix them with the extractant water at a mass ratio of 1:12 ;
[0046] (2) The extraction conditions are: extraction temperature 80°C, pH=8.5, solvent reflux rate 28% under the conditions of reflux (using 3-stage solvent circulation dynamic heat reflux) for extraction for 90 minutes;
[0047] (3) Concentration: Concentrate for 2 hours at a vacuum of 0.065MPa and a temperature of 80°C;
[0048] (4) Alcohol precipitation: add 5 times of 95% food grade or above alcohol according to the volume ratio, stir evenly and let stand for 120 minutes;
[0049] (5) Drying: Add 15 times of distilled water or other solvents to the above-mentioned alcohol precipitate according to the mass ratio and stir to dissolve i...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com