SiO2 enriched nano composite inorganic flame-retardant heat insulating thermal preserving board and manufacturing process thereof
An inorganic flame-retardant, heat-insulating and heat-insulating technology is applied in the field of inorganic composite composite sheets and their production technology, which can solve the problems of long-term drying process, limitation, waste of energy, etc., and achieves low bulk density, environmental protection in the production process, and simple production process. Effect
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Embodiment 1
[0011] SiO 2 Airgel 40g, SiO 2 23 grams of nano powder, 12 grams of zirconia superfine powder, 10 grams of glass bead material, 3 grams of expanded perlite, 1 gram of ethyltriethoxysilane, 8 grams of high modulus potassium silicate solution, silicic acid 3 grams of calcium fiber microporous slurry, the above components are dispersed, mixed, billeted, and dried for 48 hours to obtain a block with a bulk density of 89 kg / m3 and a thermal conductivity (tested by hot wire method) of 0.039w / m.k. Calcined in a muffle furnace at 1000°C for 100 hours, the weight loss was 2 wt%, and the green body was still intact.
Embodiment 2
[0013] SiO 2 Airgel 60g, SiO 2 5 grams of nano powder, 15 grams of zirconia superfine powder, 5 grams of ceramic microbead material, 3 grams of expanded perlite, 1 gram of methyltrimethoxysilane, 7 grams of tetraethylorthosilicate acidic hydrolyzate, silicic acid Aluminum magnesium fiber 4 grams. The above components are dispersed, mixed, billeted, and dried for 48 hours to obtain a block with a bulk density of 86 kg / m3 and a thermal conductivity (tested by hot wire method) of 0.038w / m.k. Calcined in a muffle furnace at 1000°C for 100 hours, the weight loss was 1.5wt%, and the green body was intact;
[0014] Calcined in the air atmosphere of a silicon carbide furnace at 1200°C for 1 hour, the weight loss was 4 wt%, and the green body was still intact.
Embodiment 3
[0016] SiO 2 Airgel 35g, SiO 2 25 grams of nano powder, 15 grams of zirconia superfine powder, 5 grams of expanded perlite, 8 grams of vermiculite, 1.5 grams of ethyl triethoxysilane, 5 grams of ethyl orthosilicate acidic hydrolyzate, aluminum phosphate solution 3 grams, magnesium aluminum silicate fiber 2.5 grams. The above components are dispersed, mixed, billeted, and dried at 80°C for 10 hours to obtain a block with a bulk density of 90 kg / m3 and a thermal conductivity (tested by hot wire method) of 0.039w / m.k. Calcined in a muffle furnace at 1000°C for 100 hours, the weight loss was 1.4wt%, and the green body was intact.
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