Foaming water discharge agent and its preparation
A foam drainage agent and raw material technology, applied in chemical instruments and methods, earthwork drilling, wellbore/well components, etc., can solve the problems of impact, shortened validity period, waste of chemicals, etc. The effect of improving work efficiency
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Embodiment 1
[0047] The consumption of each raw material component in the present embodiment foam drainage agent is as follows:
[0048] Triethylenetetramine: 5% (50kg); Diethylenetriamine: 10% (100kg); Oleic acid: 20% (200kg);
[0049] Glacial acetic acid: 2% (20kg); Maleic anhydride: 5% (50kg); Acrylic acid: 5% (50kg);
[0050] Citric acid: 2% (20kg); Imidazoline: 10% (100kg); LAS: 5% (50kg);
[0051] 20% aqueous hydrochloric acid solution in mass percent concentration: 5% (50kg);
[0052] 30% sodium hydroxide aqueous solution of mass percentage concentration: 5% (50kg);
[0053] Water: 26% (260kg).
[0054] The present embodiment foam drainage agent is prepared by the method comprising following main steps:
[0055] (1), preparation of intermediate M 1 :
[0056] Put 50kg of triethylenetetramine and 100kg of diethylenetriamine in a reaction vessel, turn on the heater, and stir while heating. When the temperature reaches 100°C, add 200kg of oleic acid and keep stirring. After adding ...
Embodiment 2
[0062] The consumption of each raw material component in the present embodiment foam drainage agent is as follows:
[0063] Triethylenetetramine: 7% (70kg); Diethylenetriamine: 10% (100kg); Oleic acid: 10% (100kg);
[0064] Glacial acetic acid: 4% (40kg); Maleic anhydride: 5% (50kg); Acrylic acid: 5% (50kg);
[0065] Citric acid: 4% (40kg); Imidazoline: 15% (150kg); LAS: 10% (100kg);
[0066] 20% aqueous hydrochloric acid solution in mass percent concentration: 5% (50kg);
[0067] 30% sodium hydroxide aqueous solution of mass percentage concentration: 5% (50kg);
[0068] Water: 20% (200kg).
[0069] The present embodiment foam drainage agent is prepared by the method comprising following main steps:
[0070] (1), preparation of intermediate M 1 :
[0071] Put 70kg of triethylenetetramine and 100kg of diethylenetriamine in a reaction vessel, turn on the heater, stir while heating, when the temperature reaches 130°C, add 100kg of oleic acid to keep the temperature between ...
Embodiment 3
[0077] The consumption of each raw material component in the present embodiment foam drainage agent is as follows:
[0078] Triethylenetetramine: 5% (50kg); Diethylenetriamine: 15% (150kg); Oleic acid: 10% (100kg);
[0079] Glacial acetic acid: 3% (30kg); Maleic anhydride: 10% (100kg); Acrylic acid: 10% (100kg);
[0080] Citric acid: 5% (50kg); Imidazoline: 10% (100kg); LAS: 7% (70kg);
[0081] 20% aqueous hydrochloric acid solution in mass percent concentration: 5% (50kg);
[0082] 30% sodium hydroxide aqueous solution in mass percent concentration: 10% (100kg);
[0083] Water: 10% (100kg).
[0084] The present embodiment foam drainage agent is prepared by the method comprising following main steps:
[0085] (1), preparation of intermediate M 1 :
[0086] Put 50kg of triethylenetetramine and 150kg of diethylenetriamine in a reaction vessel, turn on the heater, stir while heating, when the temperature reaches 110°C, add 100kg of oleic acid to keep the temperature between...
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