Film forming ability amphiphilic polymer oil layer protective agent and preparation method
An amphiphilic polymer, oil layer protection technology, applied in drilling compositions, chemical instruments and methods, etc., can solve the problems of drilling fluid infiltration into the formation, large pore pressure, no barrier layer, etc., and achieve low cost and good recovery. The effect of matching performance and reducing oil layer damage
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Embodiment 1
[0020] Embodiment 1: Pressure loss test in visible sand bed:
[0021] Screen and dry the 20-40 mesh sand and put it into the wellbore of a self-made evaluation device with an inner diameter of 15cm, and shake the surface flat. Take a certain amount of mud, add self-made amphiphilic polymer oil layer protection agent, after high-speed shearing and stirring to dissolve, slowly pour into the fluid loss evaluation device, pressurize 7.5 kg with nitrogen, and keep the pressure for 7.5 minutes. In this experiment, based on mud volume, the amount of oil layer protective agent added is 1%, 2%, and 3% of the mud volume respectively, and the fluid loss of pure mud without oil layer protective agent is measured, and four sets of data are measured for comparison.
[0022] Synthetic formula 1: Add refined butyl acrylate, 2-acrylamide-2-methylpropanesulfonic acid, aqueous solution of sodium acrylamide alkylsulfonate and chlorinated polyvinyl alcohol (PEG-Cl) into a container with a rotor A...
Embodiment 2
[0031] Embodiment 2, the present invention is prepared according to the formula described in Embodiment 1, and the dehydration experiment at high temperature and high pressure is as follows:
[0032] (1) The preparation density is 1.03g cm -3 Base slurry: add 3% sodium bentonite to water, then add 0.24% anhydrous sodium carbonate, stir at high speed for 20 minutes, and maintain at room temperature for 24 hours before use.
[0033] (2) Measure 200 mL of the base slurry, select the oil reservoir protection agent prepared by formula 2, add it to the base slurry at a volume fraction of 2%, and stir evenly.
[0034] (3) Measure the fluid loss. The measurement conditions are: 70°C, 3.5MPa, 30min. The filter paper used is standard filter paper, and the fluid loss reduction effect is shown in Table 1:
[0035] Table 1 Water loss at high temperature and high pressure according to formula 2 with different additions
[0036]
[0037] Note: AV: apparent viscosity; PV: plastic visco...
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