Environment-friendly water-based conductive black slurry for coatings and preparation method thereof
An environmentally friendly, water-based technology, applied in dyeing, textiles and papermaking, etc., can solve the problems of poor water resistance, flame retardancy, poor acid and alkali resistance, non-foldable use, and poor hand feeling, so as to achieve good adhesion and improve Air permeability, cost reduction effect
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Embodiment 1
[0026] Mix 29.6kg of water, 20kg of 25% aliphatic polyoxyethylene ether aqueous solution, 2.0kg of triethanolamine, 2.0kg of anionic alkyl polyoxyethylene ether sodium sulfate, and 35kg of nano-scale conductive carbon black for wetting and pre-dispersion, and stir for 1 hour , the stirring speed is 1000 rev / min, and the soaked raw material is obtained.
[0027] Stir 0.1kg of methylisothiazolinone, 0.2kg of organosilicon defoamer, 0.1kg of carbendazim, 8kg of diethylene glycol and 3kg of nonionic phenolic derivative dispersant for 0.5h, The stirring speed is 800 rev / min, and high-speed dispersion of mixing aids is obtained.
[0028] Then add the high-speed dispersed mixing aid into the stirred soaking raw material, the stirring time is 0.5h, and the stirring speed is 1200 rpm. Then use a vertical sand mill for sand grinding at a speed of 400L / h until the particle size reaches below 10um to obtain an environmentally friendly water-based black slurry with good electrical conduct...
Embodiment 2
[0030] Mix 38.6kg of water, 10kg of 25% aliphatic polyoxyethylene ether aqueous solution, 4.0kg of triethanolamine, 4.0kg of anionic alkyl polyoxyethylene ether sodium sulfate, and 35kg of nano-scale conductive carbon black for wetting and pre-dispersion, and stir for 1 hour , the stirring speed is 1000 rev / min, and the soaked raw material is obtained.
[0031] With 0.1kg of methylisothiazolinone, 0.2kg of silicone defoamer, 0.1kg of n-octylisothiazolinone, 4kg of diethylene glycol and 4kg of nonionic phenolic derivative dispersant, first stir, Stir for 0.5h, and the stirring speed is 800 rpm to obtain a high-speed dispersed mixing aid.
[0032] Then add the high-speed dispersed mixing aid into the stirred soaking raw material, the stirring time is 0.5h, and the stirring speed is 1200 rpm. Then use a vertical sand mill for sand grinding at a speed of 400L / h until the particle size reaches below 10um to obtain an environmentally friendly water-based black slurry with good elec...
Embodiment 3
[0034] Mix 50.6kg of water, 13kg of 25% aliphatic polyoxyethylene ether aqueous solution, 2.0kg of triethanolamine, 4.0kg of anionic emulsifier, and 35kg of conductive carbon black for wetting and pre-dispersion, and stir for 1 hour at a stirring speed of 1000 rpm , to obtain the infiltrated raw material.
[0035] Stir 0.1kg of methylisothiazolinone, 0.2kg of silicone defoamer, 0.1kg of n-octylisothiazolinone, 4kg of diethylene glycol and 6.0kg of nonionic phenolic derivative dispersant , stirred for 0.5h, and the stirring speed was 800 rpm to obtain a high-speed dispersion of the mixing aid.
[0036] Then add the high-speed dispersed mixing aid into the stirred soaking raw material, the stirring time is 0.8h, and the stirring speed is 1200 rpm. Then use a vertical sand mill for sand grinding at a speed of 400L / h until the particle size reaches below 10um to obtain an environmentally friendly water-based black slurry with good electrical conductivity.
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