Conductive fiber preparation method and product thereof
A technology of conductive fibers and conductive materials, applied in fiber types, fiber processing, textiles and papermaking, etc., can solve the problems of complex polymer synthesis mechanism, difficult spinning process, toxic polymer monomers, etc. It is easy to achieve industrialization , long-lasting conductivity and controllable conductivity
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preparation example Construction
[0026] 1. Preparation of photosensitive polymer:
[0027] 1. Preparation of macromolecular photosensitizer:
[0028] Add an appropriate amount of 2,4 dihydroxybenzophenone (UV-0) and a weight ratio of 0.8% to 2% NaOH into a dry three-necked flask, fill with nitrogen for 30 minutes, then add glycidyl methacrylate ( GMA), (the molar ratio to UV-0 is 1:1~2:1), stirring and heating up to 60°C-90°C, the reaction time is 3h-8h, to obtain a yellow viscous liquid (BPMA), keep away from light for later use .
[0029] 2. Preparation of photosensitive polymer:
[0030] Add polymer monomers N-vinylpyrrolidone (VP) and BPMA (wherein the amount of VP and BPMA can be 10% to 90% of the total molar amount of both) in the three-necked flask, add an appropriate amount of deionized water, add Sodium dodecyl sulfate (SDS) with a weight ratio of 1% to 10%, adding 1% to 5% azobisisobutylcyanide (AIBN) as an initiator, nitrogen gas for 30 minutes, stirring, reflux, and reaction temperature 50℃~80...
Embodiment 1
[0043] 1. Preparation of photosensitive polymer:
[0044] 1. Preparation of macromolecular photosensitizer:
[0045] Add 10.7g of 2,4 dihydroxybenzophenone (UV-0) and 0.155g of NaOH into a dry three-necked flask, fill with nitrogen for 30 minutes, then add 7.9g of glycidyl methacrylate (GMA), (with UV The molar ratio of -0 is 1:1), the temperature was raised to 80° C. with stirring, and the reaction time was 5 h to obtain a yellow viscous liquid (BPMA), which was kept away from light for use.
[0046] 2. Preparation of photosensitive polymer:
[0047] 33gN-vinylpyrrolidone (VP) and 12gBPMA (wherein the consumption of VP and BPMA accounts for both molar totals are respectively 90%, 10%) in the there-necked flask respectively, add an appropriate amount of deionized water, adding a weight ratio of 1.7g ( 4wt% sodium dodecyl sulfate (SDS), add 0.48g (2wt%) azobisisobutylcyanide (AIBN), blow nitrogen for 30 minutes, stir, reflux, reaction temperature 80°C, reaction time 3h. Afte...
Embodiment 2
[0054] 1. Preparation of photosensitive polymer:
[0055] 1. Preparation of macromolecular photosensitizer:
[0056] Add 10.7g of 2,4 dihydroxybenzophenone (UV-0) and 0.212g of NaOH into a dry three-necked flask, fill with nitrogen for 30 minutes, then add 15.8g of glycidyl methacrylate (GMA), (with UV The molar ratio of -0 is 2:1), and the temperature was raised to 60°C with stirring, and the reaction time was 3 hours to obtain a yellow viscous liquid (BPMA), which was kept away from light for use.
[0057] 2. Preparation of photosensitive polymer:
[0058] 3.7gN-vinylpyrrolidone (VP) and 108gBPMA (wherein the consumption of VP and BPMA accounted for 10% and 90% respectively of the total moles of the two) in the three-necked flask respectively, added an appropriate amount of deionized water, adding a weight ratio of 1.17g (1wt%) sodium dodecyl sulfate (SDS), add 1.17g (1wt%) ammonium persulfate (APS), nitrogen flow for 30 minutes, stir, reflux, reaction temperature 50 ° C, ...
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