Chemical plating method for quartz fiber surface
A technology of surface chemistry and quartz optical fiber, which is applied in the field of chemical nickel-phosphorus-boron alloy plating on the surface of quartz optical fiber, which can solve the problems that the surface hardness and conductivity of optical fiber cannot meet higher requirements.
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[0004] 1. Optical fiber surface pretreatment: Use 30% sodium hydroxide solution by volume to remove organic matter on the optical fiber surface, wash with deionized water, roughen in hydrofluoric acid and ammonium fluoride solution, then wash with distilled water, dry, and finally immerse for activation Optionally, use V(40%HF):V(H2SiF6):V(H2O) = 1:1:2 to weaken in the crude solution for 10 minutes and 20 minutes respectively.
[0005] 2. The plating solution is composed of nickel chloride hexahydrate 24g / L, sodium hypophosphite 10g / L, potassium borohydride 10g / L, ethylenediamine 24mL / L, cadmium sulfate 0.6mg / L, pH=13-14, temperature 90°C, perform electroless plating on the prepared optical fiber.
[0006] The cross-sectional morphology of the electroless plating surface was observed with a scanning electron microscope, and the composition of the coating was measured with an energy spectrometer, a plasma emission spectrometer, XRD and other equipment and various conventional a...
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