Method for preparing TiB2 cathode coating for aluminium electrolysis
A cathode coating and aluminum electrolysis technology, which is applied in the field of preparation of TiB2 cathode composite coating materials for aluminum electrolytic cells, can solve the problems of inability to realize large-scale production, difficulty in applying aluminum electrolysis production, and high cost of cathode products, and achieve production processing Low cost, improved electrolytic current efficiency, and reduced labor intensity
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Embodiment 1
[0019] According to TiB 2 Weight percent content of coating composite, TiB 2 , petroleum coke and carbon fiber were crushed and ball-milled several times to obtain a solid powder with a particle size of 10-50 μm, and put it in the kneading equipment at a ratio of 20:50:3 by weight, start the kneader, and mix for 2 hours to obtain a uniform solid powder mix. Fully mix the weighed asphalt and acetone in the container according to the ratio of 20:7 by weight to obtain a mixture with certain fluidity, pour it into the kneading equipment for solid-liquid kneading for 5 hours, and control the kneading temperature to 50°C . Obtain the TiB needed for aluminum electrolysis 2 composite material.
[0020] The composite material is hand-applied on the surface of the cathode carbon block of the entire electrolytic cell, smoothed and cured. The composite-coated cathode cell is then applied to the electrolytic aluminum system.
[0021] Implementation results: 25°C, TiB 2 The electrica...
Embodiment 2
[0023] According to TiB 2 Weight percent content of coating composite, TiB 2 , metallurgical coke, and carbon fiber were crushed to 10-30 μm by crushing ball mill several times, and put in the kneading equipment according to the ratio of 25:43:5 by weight. Start the kneader and mix for 3 hours to obtain a uniform solid powder mixture. After the phenolic resin and diethylenetriamine are fully stirred and mixed in the container according to the ratio of 22:5 by weight, a mixture with certain fluidity is obtained, which is poured into the kneading equipment for solid-liquid kneading for 10 h, and the kneading temperature is controlled at 80 ℃. Obtain the TiB needed for aluminum electrolysis 2 composite material.
[0024] The composite material is hand-applied on the surface of the cathode carbon block of the entire electrolytic cell, smoothed and cured. The composite-coated cathode cell is then applied to the electrolytic aluminum system.
[0025] Implementation results: 25°...
Embodiment 3
[0027] According to TiB 2 Weight percent content of coating composite, TiB 2 1. Electric calcined anthracite is crushed to 10-80 μm by crushing ball mill for several times, and placed in the kneading equipment according to the ratio of 30:43 by weight. Start the kneader and mix for 2 hours to obtain a uniform solid powder mixture. Anthracene oil and ethanol were fully stirred and mixed in a container according to the ratio of 26:1 by weight to obtain a mixture with certain fluidity, which was poured into a kneading equipment for solid-liquid kneading for 18 h, and the kneading temperature was controlled at 40 °C. Obtain the TiB needed for aluminum electrolysis 2 composite material.
[0028] The composite material is hand-applied on the surface of the cathode carbon block of the entire electrolytic cell, smoothed and cured. The composite-coated cathode cell is then applied to the electrolytic aluminum system.
[0029] Implementation results: 25°C, TiB 2 The electrical cond...
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