Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Polysilicon ingot casting method with low defect and high output and thermal field structure thereof

A polysilicon, low-defect technology, applied in the growth of polycrystalline materials, chemical instruments and methods, crystal growth, etc., can solve the problems of high grain boundary and dislocation defect density, low solar cell efficiency, and insignificant cost advantages. Improve crystal quality, reduce energy consumption, and facilitate the effect of adjusting the crystal growth interface

Active Publication Date: 2012-01-25
TRINA SOLAR CO LTD
View PDF3 Cites 26 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The high energy consumption is mainly due to the position of the heater in the upper half of the entire thermal field structure. The heater is located on the top and upper side of the thermal field. In order to maintain the temperature gradient of crystal growth, more energy is lost.
At present, the 450kg polycrystalline ingot furnace type is generally used in the industry. Due to the problem of production capacity or the load of the slicer, the actual feeding amount is generally 390-420kg. With the development of the industry, the competition is becoming more and more fierce, and the solar cell manufacturers are getting more and more More and more attention is paid to cost control. In order to increase production capacity and reduce energy costs, various new equipment are constantly being developed. The polycrystalline furnace has a larger furnace type (800kg) successfully developed, and these large furnace types are developing horizontally. , that is, the original 450kg polycrystalline ingot furnace type can cut 25 small pieces of 156mm×156mm×250mm, and the 800kg furnace type can cut 36 such small pieces, but the large-scale crucible production process is not yet mature. , and require a larger square cutting machine, the original square cutting machine is too narrow to continue to use, so its cost advantage is not obvious
In order to improve the output, on the basis of the original 450kg furnace type, the charging amount is directly increased. With the increase of the charging amount, it is difficult to dissipate heat in the later stage of crystal growth, the crystal growth time is greatly prolonged, and the energy consumption is increased.
At the same time, due to the problem of the growth method of the polysilicon ingot, the bottom of the quartz ceramic crucible starts to dissipate heat first, and the heat dissipation intensity of the entire plane is basically the same. Many nucleation points are generated at the bottom of the crucible, and the resulting grains are small, and the density of grain boundaries and dislocation defects Higher, so compared with single crystal, the solar cell efficiency will be lower by 1% to 2%

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Polysilicon ingot casting method with low defect and high output and thermal field structure thereof
  • Polysilicon ingot casting method with low defect and high output and thermal field structure thereof
  • Polysilicon ingot casting method with low defect and high output and thermal field structure thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] After the quartz crucible 12 is filled with 650kg of silicon material, the outsourcing graphite crucible 6 is placed on the support block 7, the side wall 5 of the insulation cover and the lower insulation plate 9 are closed, and the distance between the top heater 2 and the support block 7 reaches 650mm. The furnace body is evacuated, and after the vacuum degree required by the process is reached, the top heater 2, the side heater 3 and the side heater 4 start to work. After initial preheating, the inert protective gas argon is gradually introduced through the protective gas introduction pipe 14, The pressure in the furnace is maintained at 0.5 atm. Due to the heat preservation effect of the heat preservation cover, the temperature in the heat preservation cover can be raised to a high temperature of about 1500°C, so that the silicon material can be heated and melted within more than ten hours. The argon gas that circulates during the materialization can carry the impur...

Embodiment 2

[0030] After the quartz crucible 12 is filled with 750kg of silicon material, the outsourcing graphite crucible 6 is placed on the support block 7, the side wall of the heat preservation cover 5 and the lower insulation plate 9 are closed, and the distance between the top heater 2 and the support block 7 reaches 700mm. The furnace body is evacuated, and after the vacuum degree required by the process is reached, the top heater 2, the side heater 3 and the side heater 4 start to work. After initial preheating, the inert protective gas argon is gradually introduced through the protective gas introduction pipe 14, The pressure in the furnace is maintained at 0.6atm. Due to the heat preservation effect of the heat preservation cover, the temperature in the heat preservation cover can be raised to a high temperature of about 1500°C, so that the silicon material can be heated and melted within more than ten hours. The argon gas that circulates during the materialization can carry the...

Embodiment 3

[0035] Quartz crucible 12 first lays a strip-shaped crystal-oriented single crystal with a certain thickness at the position corresponding to the cooling point of the support block at the bottom of the crucible, and then fills it with 650kg of silicon material, outsources the graphite crucible 6, and places it on the support block 7, and the support block 7 With 4 strip cooling spots, such as image 3 , the insulation cover side wall 5 and the lower insulation board 9 are closed, the distance between the top heater 2 and the support block 7 reaches 650mm, the furnace body is evacuated, and after reaching the vacuum degree required by the process, the top heater 2 and the side heater 3 and side lower heater 4 start to work, and after the initial preheating, the inert protective gas argon is gradually introduced through the protective gas introduction pipe 14 to maintain the pressure in the furnace at 0.4 atm. After rising to a high temperature of 1400°C, lift the heat preserva...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to a polysilicon ingot casting method with low defect and high output and a thermal field structure thereof. The thermal field structure comprises a thermal insulation cover system, a crucible system, split resistance heaters, a support part and a cooling device, wherein the three heaters are independently and separably controlled to lower energy consumption to the maximum degree and bring convenience for regulating a crystal growth interface, thereby obtaining an evener crystal growth interface, improving crystal quality and solving the later-stage cooling problem of the crystal growth because of the increase of the height of the ingot casting. A support block with the unique design and a cooling device are combined to realize the purpose of local cooling, so that the local position on the bottom of a crucible generates cold spots at the early stage of the crystal growth; nucleation is carried out firstly to reduce nucleation spots, and lateral temperature gradient is obtained to provide the necessary condition for the lateral growth of the crystal nucleus; crystalline grains are enlarged to reduce a crystal boundary to the large extent; and microdefects, such as dislocation and the like, are lowered.

Description

technical field [0001] The invention belongs to the technical field of solar cell ingot casting, and relates to a low-defect high-yield polycrystalline silicon ingot casting method and a thermal field structure thereof. Background technique [0002] In the field of solar photovoltaics, the method of directional solidification to produce polysilicon ingots is a commonly used method. The basic principle is: place the polysilicon raw material in a quartz ceramic crucible, place it in a specific thermal field system, and heat it until it is completely melted; The bottom of the crucible begins to cool, and the silicon solution begins to crystallize at the bottom of the crucible and gradually grows (solidifies); The consumption is around 3800 degrees. The high energy consumption is mainly due to the fact that the heater is located in the upper half of the entire thermal field structure. The heater is located at the top and upper side of the thermal field. In order to maintain the...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C30B28/06C30B29/06
Inventor 陈雪
Owner TRINA SOLAR CO LTD
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products