Slowly-released peroxide initiating system with nano structure and preparation method thereof
A technology of peroxide and nanostructure, which is applied in the field of slow-release peroxide initiation system and its preparation, can solve the problems of difficulty in free radical diffusion, difficulty in increasing grafting rate, and difficulty, and achieve broad application prospects and industrial value , slow down the generation rate, and avoid the effect of excessive concentration
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Embodiment 1
[0024] 60% organically modified nano-montmorillonite was dispersed in 100ml of acetone; 1% DCP was dissolved in 20ml of acetone, and then slowly added dropwise to the montmorillonite suspension at room temperature, stirring while adding; 39%Nd 2 o 3 , and stirred evenly; then placed in a vacuum oven, dried at 40° C. for 24 hours to obtain the product 1 of the initiating system.
Embodiment 2
[0026] 70% organically modified nano-montmorillonite was dispersed in 100ml of acetone, and subjected to 200W ultrasonic treatment for 1h; 20% DCP was dissolved in 20ml of acetone, and then slowly added dropwise to the montmorillonite suspension at room temperature, while adding While stirring; add 10% Nd to the solution 2 o 3 , stirred evenly; then placed in a vacuum oven, dried at 40° C. for 24 hours to obtain the product 2 of the initiator system.
Embodiment 3
[0028] 76% organically modified nano-montmorillonite was dispersed in 100ml of acetone, and subjected to 200W ultrasonic treatment for 1h; 2% DCP was dissolved in 20ml of acetone, and then slowly added dropwise to the montmorillonite suspension at room temperature, while adding While stirring; add 22% CeO to the solution 2 , stirred evenly; then placed in a vacuum oven and dried at 40°C for 24 hours to obtain the product 3 of the initiating system.
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