Water-based environment-friendly electrostatic spraying baking paint and preparation method thereof
An electrostatic spraying, environmental protection technology, applied in the direction of coating, etc., to achieve the effect of high hardness, solve safety and environmental protection problems, and plump paint film
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[0033] A kind of preparation method of water-based environment-friendly electrostatic spraying baking varnish, it comprises the following steps
[0034] A) preparation of modified water-based resin:
[0035] (1) Add epoxy resin, ethylene glycol butyl ether, isopropanol, and propylene glycol methyl ether into the reaction kettle in proportion, turn on the mixer and stir for 10-15 minutes, set the temperature of the reaction kettle to 113-118°C, and start heating ;
[0036] (2) Put butyl acrylate, hydroxypropyl acrylate, methyl acrylate, acrylic acid and initiator into the mixing tank in proportion to mix, and after mixing evenly, let it stand for 20-40 minutes to obtain the mixed material;
[0037] (3) Put the above-mentioned mixed material into the high-level dripping tank;
[0038] (4) When the temperature in the reactor rises to the set value and reflux begins, start to add the above-mentioned mixed material dropwise, and the dropping time is controlled at 3-4 hours, and t...
Embodiment 1
[0046] The preparation method of water-based environment-friendly electrostatic spraying baking paint comprises:
[0047] A) Preparation of modified water-based resin: add 15% of epoxy resin, 11% of ethylene glycol butyl ether, 8% of isopropanol, and 12% of propylene glycol methyl ether into the reaction kettle in proportion according to the mass percentage, turn on the mixer and stir for 10 minutes, Set the temperature of the reaction kettle to 115°C and start heating; then put 13% butyl acrylate, 11% hydroxypropyl acrylate, 6% methyl acrylate, 8% acrylic acid and 3% initiator into the mixing tank in proportion to mix , After mixing evenly and standing for 30 minutes, the obtained mixed material was poured into the high-level dripping tank; when the temperature in the reactor rose to the set value and began to reflux, the above-mentioned mixed material was started to be added dropwise, and the dropping time was controlled at 3 hours. The temperature of the reaction kettle is ...
Embodiment 2
[0052]A) Preparation of modified water-based resin: add 10% of epoxy resin, 10% of ethylene glycol butyl ether, 10% of isopropanol, and 15% of propylene glycol methyl ether into the reaction kettle in proportion according to the mass percentage, turn on the mixer and stir for 10 minutes, Set the temperature of the reaction kettle to 113-118°C and start heating; then add 15% butyl acrylate, 15% hydroxypropyl acrylate, 10% methyl acrylate, 10% acrylic acid and 2% initiator into the mixture in proportion Tank mixing, after mixing evenly and standing for 20 minutes, the mixed material was put into the high-level dripping tank; when the temperature in the reactor rose to the set value and began to reflux, the above-mentioned mixed material was started to be added dropwise, and the dropping time was controlled at 3 Hours, the temperature of the reaction kettle is controlled at 118°C; after the dropwise addition, keep warm for 3 hours, measure the acid ester, when the acid value is 60...
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