Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Oil-water separating mesh film and preparation method thereof

An oil-water separation mesh membrane and phase separation technology, applied in separation methods, liquid separation, chemical instruments and methods, etc., can solve the problems of complex preparation process, difficult to degrade, difficult to handle, etc., and achieve the effect of high separation efficiency

Active Publication Date: 2012-10-03
TSINGHUA UNIV
View PDF5 Cites 34 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although these separation membranes have achieved the effect of oil-water separation, they all have certain shortcomings.
Some preparation processes are complicated, some use fluorine-containing organic substances, and some need to add a variety of chemical reagents. At the same time, the preparation of these oil-water separation membranes needs to be supported by other fabrics such as steel mesh, copper mesh, and nylon mesh. The production cost is increased. At the same time, the materials used for the oil-water separation membrane itself are mostly chemically synthesized polymer materials, which are not easy to degrade. The lipophilicity of the material itself makes the membrane very easy to be polluted by oil. The use of incineration and landfill treatment methods will cause secondary pollution to the environment and other issues.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Oil-water separating mesh film and preparation method thereof
  • Oil-water separating mesh film and preparation method thereof
  • Oil-water separating mesh film and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0040] Embodiment 1, the preparation of oil-water separation omentum

[0041] 1. Dissolve PLA (polylactic acid, Shenzhen Guanghua Weiye Industrial Co., Ltd., molecular weight = 69000, L-polylactic acid) in 1,4-dioxane solvent to prepare a PLA solution with a concentration of 0.1g / mL, and take 4ml PLA solution, then add sodium chloride crystals (0.15g, the mass ratio of PLA and sodium chloride is 8:3), stir to form a uniform mixture, then spread the mixture evenly on the glass substrate, and let it stand in the air for 3min (to make the PLA solution flat), then immerse the glass substrate covered with the mixed solution in absolute ethanol, and perform phase separation for 30 minutes to form a film;

[0042] 2. Take out the above-mentioned glass substrate with film and immerse it in water again to remove the porogen sodium chloride, take it out after 10 hours and put it in an oven to dry at 40°C to obtain an oil-water separation omentum.

Embodiment 2

[0043] Embodiment 2, the characteristic and functional identification of oil-water separation omentum

[0044] 1. Electron microscope scanning observation aperture

[0045] The oil-water separation omentum obtained in the above 1 was scanned with an electron microscope, and the surface morphology was observed at a magnification of 9900 times. The results are as follows figure 1 As shown, it can be seen that there is a micro-nano composite porous structure, which can be observed at 460 times magnification as figure 2 As shown, it can be seen that the omentum has a macroporous structure of 50nm-300um under the action of sodium chloride, the largest pore diameter can reach 300um, and the smallest pore diameter is only 50nm.

[0046] 2. Research on oil absorption and hydrophobicity of oil-water separation omentum

[0047] In the air, drop 2 microliters of water on the oil-water separation membrane obtained in the above 1, and use a contact angle measuring instrument, the result...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses an oil-water separating mesh film and a preparation method thereof. The preparation method comprises the following steps of: 1) dissolving polylactic acid in an organic solvent to obtain a polylactic acid solution; 2) adding a porogen into the polylactic acid solution and evenly mixing to obtain a mixed solution; and 3) carrying out phase separation on the mixed solution, so as to obtain the oil-water separating mesh film. The experiment of the invention proves that the oil-water separating mesh film disclosed by the invention has the characteristics of stability and high separation efficiency; the oil-water separating mesh film can be prepared in large area, the separated oil can be recycled, the separating mesh film can be repeatedly used, and the separation effect can not be influenced. After being used and abandoned, the oil-water separating mesh film can be degraded in the natural environment, so that the secondary pollution can be avoided. The biodegradable oil-water separating mesh film with super-hydrophobic and super-oleophylic properties can be used for oil-water separation of oily sewage containing edible oil, gasoline and the like.

Description

technical field [0001] The invention belongs to the technical fields of chemical engineering and functional materials, and in particular relates to an oil-water separation membrane and a preparation method thereof. Background technique [0002] With the massive discharge of oily sewage in production and life and the frequent occurrence of oil spill accidents at sea, the exploration and research of oil-water separation has become an important topic related to people's life, economic development and environmental safety, and oil-water separation technology is very important for solving water pollution and Issues such as the purification of fuel oil play a vital role. Traditional oil-water separation methods such as gravity separation, centrifugal separation, electrical separation, adsorption separation, and air flotation separation have many disadvantages. Some separation efficiency is not high, and some chemicals are added too much to cause secondary pollution. Some energy c...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): B01D17/022
Inventor 冯琳孙中雪薛众鑫陈雨宁卢飞刘娜高常锐张诗妍危岩
Owner TSINGHUA UNIV
Features
  • Generate Ideas
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More