Preparation method for cobalt carbonate material with dense structure and globoid shape
A sphere-like, cobalt carbonate technology, applied in cobalt carbonate and other directions, can solve the problems of disordered morphology, loose microstructure of cobalt carbonate materials, poor uniformity, etc., and achieve better structure compactness, easy control of process parameters, and better particle size distribution. Effect
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[0022] Example 1
[0023] Put a cobalt chloride solution with a cobalt concentration of 1.0 mol / L and a pH value of 4.75 into the reactor after filtration;
[0024] Under stirring conditions, heating steps Solution, control the temperature of the solution system at 55℃ and keep the system temperature relatively stable;
[0025] Spray the pre-filtered ammonium bicarbonate solution with a concentration of 1.8 mol / L at a flow rate of 800L / h to the step In the system;
[0026] Control steps The pH value of the medium solution system is 7.5 as the end point of the system reaction, that is, the addition of ammonium bicarbonate solution is terminated;
[0027] Steps The obtained solid-liquid system is aged for 20 minutes, filtered, and washed repeatedly to obtain the desired material.
[0028] The spheroid morphology and particle size distribution of the material prepared in Example 1 are as figure 1 with figure 2 , The physical index "measurement result of particle size and density" ...
Example Embodiment
[0029] Example 2
[0030] Put a cobalt chloride solution with a cobalt concentration of 1.5 mol / L and a pH value of 4.80 into the reactor after filtration;
[0031] Under stirring conditions, heating steps Solution, control the temperature of the solution system at 63℃, and keep the system temperature relatively stable;
[0032] Spray the pre-filtered ammonium bicarbonate solution with a concentration of 2.0 mol / L at a flow rate of 588L / h to the step In the system;
[0033] Control steps The pH value of the medium solution system is 7.2 as the end point of the system reaction, that is, the addition of ammonium bicarbonate solution is terminated;
[0034] Steps The obtained solid-liquid system is aged for 30 minutes, filtered, and washed repeatedly to obtain the desired material.
[0035] The spheroid morphology and particle size distribution of the material obtained in Example 2 are as image 3 with Figure 4 , The physical index "measurement result of particle size and density...
Example Embodiment
[0036] Example 3
[0037] Put a cobalt chloride solution with a cobalt concentration of 1.6 mol / L and a pH value of 5.09 into the reactor after filtration;
[0038] Under stirring conditions, heating steps Solution, control the temperature of the solution system at 60℃ and keep the system temperature relatively stable;
[0039] Spray the pre-filtered ammonium bicarbonate solution with a concentration of 1.86 mol / L at a constant rate of 280L / h to the step In the system;
[0040] Control steps The pH value of the medium solution system is 7.2 as the end point of the system reaction, that is, the addition of ammonium bicarbonate solution is terminated;
[0041] Steps The obtained solid-liquid system is aged for 30 minutes, filtered, and washed repeatedly to obtain the desired material.
[0042] The spheroid morphology and particle size distribution of the material prepared in Example 3 are as Figure 5 with Image 6 , The physical index "measurement result of particle size and dens...
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