Polybutylece terephthalate (PBT) coated functional powder and preparation method thereof
A functional powder, powder technology, applied in fibrous filler, dyed low molecular organic compound treatment, dyed high molecular organic compound treatment and other directions, can solve the problems of complex treatment technology, narrow applicability, etc. Universal, easy-to-use effects
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Embodiment 1
[0047] (1) Carry a layer of CBT catalyst on the surface of nano-titanium dioxide: dissolve the catalyst ethyl titanate in ethanol to form a solution with a mass concentration of 25%, then add nano-titanium dioxide to the above solution, and carry out Stir, the ethyl titanate will be fully coated on the surface of the nano-titanium dioxide, the particle size of the nano-titanium dioxide is 20nm, and the mass ratio of the nano-titanium dioxide to the ethyl titanate in the solution is 15:1; , to obtain the lower precipitate, and further remove the ethanol solvent at 90°C to obtain the loaded nano-titanium dioxide loaded with ethyl titanate;
[0048] (2) Preparation of mixed powder: mix CBT powder with the above-mentioned nano-titanium dioxide loaded with ethyl titanate, the mass ratio of the CBT to the nano-titanium dioxide is 2:1; dry the mixed powder ;
[0049] (3) In-situ polymerization: After in-situ polymerization and spray powdering of the dried mixed powder, PBT-coated na...
Embodiment 2
[0051] (1) Carry a layer of CBT catalyst on the surface of tourmaline powder: dissolve the catalyst ethyl titanate in ethanol to form a solution with a mass concentration of 25%, and then add tourmaline powder to the above solution and stirring, the ethyl titanate will be fully coated on the surface of the tourmaline powder, the particle size of the tourmaline powder is 20nm, the mass ratio of the tourmaline powder to the ethyl titanate in the solution The ratio is 15:1; standing for stratification, obtaining the lower layer of precipitation, further removing the ethanol solvent at 90°C, and obtaining the loaded tourmaline powder loaded with ethyl titanate;
[0052] (2) Preparation of mixed powder: mix CBT powder with the above-mentioned tourmaline powder loaded with ethyl titanate, the mass ratio of the CBT to the tourmaline powder is 2:1; The powder is dried;
[0053] The specific steps of mixing as mentioned above are:
[0054] a) Put CBT into a high-speed pulverizer to m...
Embodiment 3
[0062] (1) Carry a layer of CBT catalyst on the surface of the phosphor: dissolve the catalyst isopropyl titanate in ethanol to form a solution with a mass concentration of 35%, and then add the phosphor to the above solution , and stirring, isopropyl titanate will be fully coated on the surface of the phosphor, the particle size of the phosphor is 80nm, and the mass ratio of the phosphor to isopropyl titanate in the solution is 25 : 1; standing for stratification, obtaining the lower layer of precipitation, further removing the ethanol solvent at 100°C, and obtaining the loaded phosphor body loaded with isopropyl titanate;
[0063] (2) Preparation of mixed powder: mix CBT powder with the above-mentioned phosphor loaded with isopropyl titanate, the mass ratio of the CBT to the phosphor is 4:1; the mixed The powder is dried;
[0064] The specific steps of mixing as mentioned above are:
[0065] a) Put CBT into a high-speed pulverizer to make CBT powder. The pulverization oper...
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