Processing method of salt-free dyeing through activated dye
A reactive dye and salt-free dyeing technology, applied in dyeing methods, textiles and papermaking, etc., can solve the problem of high direct dye fixation rate or high price of dye fastness, affecting fabric shade and level dyeing, dyeing level dyeing Difficult to overcome and other problems to achieve the effect of avoiding environmental and ecological problems, simplifying labor intensity, and improving the equilibrium adsorption capacity
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Embodiment 1
[0029] 1. Mercerized cotton (40 s / 2) Pre-treatment of line cooking and bleaching: the cooking and bleaching process is: H 2 o 2 (27%) 5.5g / L, NaOH (50%) 3.0g / L, multifunctional scouring agent SSS (Shanghai Yayun) 1.5g / L, liquor ratio 1:10, temperature 110°C, time 20min, then pickling , enzyme washing;
[0030] 2. Prepare a mixed solution of water and absolute ethanol: under normal temperature conditions, add water and absolute ethanol in a volume ratio of 1:9 to the sealed cheese dyeing machine equipped with fabrics, the bath ratio is 1:10, and adjust the pH to 7.5± 0.1;
[0031] 3. High-temperature reactive red HE3B salt-free dyeing: dye dosage 1% (o.w.f), dyeing at 30°C for 20 minutes, then add soda ash 10g / L at one time, heat up to 60°C at 1°C / min, and keep warm for 30 minutes;
[0032] 4. Post-treatment of dyed yarn: After dyeing, the yarn is washed with water, pickled, soaped (soaping agent AST 1g / L, temperature 95°C, time 15 minutes), hot water washing, color fixing...
Embodiment 2
[0039] 1. Cotton wool (50 s / 1) Pretreatment before cooking and bleaching: the cooking and bleaching process is: H 2 o 2 (27%) 5.5g / L, NaOH (50%) 3.0g / L, multifunctional scouring agent SSS (Shanghai Yayun) 1.5g / L, liquor ratio 1:20, temperature 95°C, time 30min, then pickling , enzyme washing;
[0040] 2. Prepare a mixed solution of water and acetone: at room temperature, add water and acetone in a volume ratio of 1:4 into the sealed dyeing machine equipped with cotton wool, the bath ratio is 1:20, and adjust the pH to 7.5±0.1;
[0041] 3. Medium-temperature reactive black B salt-free dyeing: dye dosage 5% (o.w.f), dyeing at 30°C for 20 minutes, then linearly add soda ash 20g / L within 20 minutes, heat up to 50°C at 1°C / min, and keep warm for 60 minutes ;
[0042] 4. Post-treatment of dyed yarn: After dyeing, the yarn is washed with water, pickled, soaped (soaping agent AST 2g / L, temperature 95°C, time 20 minutes), hot water washing, color fixing and softness (color fixing ...
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