Method for producing calcium formate from sugar mill filter mud
A sugar factory filter sludge and calcium formate technology, which is applied in the direction of carboxylate preparation, etc., can solve the problems of carbonation filter sludge moisture and organic nutrients not reaching biological fertilizers, difficulty in consuming filter sludge, waste of land resources, etc., to achieve promotion Effects of sustainable development, improvement of competitiveness, and reduction of economic pressure
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[0021] Main raw materials and specifications: formic acid content 88.0%, heavy metal (calculated as Pb) ≤ 0.0003% diluted to 70%, spare; equipped with 25% (mass volume ratio) lime milk solution, spare; filter mud calcium carbonate content ≥ 70%, fine Degree 200 mesh, moisture content ≤ 18%, PH: 7~8.
[0022] The bulk particles of the filter mud are crushed, and the crushed raw material filter mud calcium carbonate powder is added to the reaction tank, and then the prepared formic acid solution is added, and the stirring is started. At room temperature, formic acid is added dropwise to the reaction tank until the pH is 4. , and then continue to react for 20 minutes until no bubbles are generated to ensure that the calcium carbonate in the filter mud reacts completely. Then add 25% milk of lime to carry out neutralization reaction of excess formic acid, react until the pH value is 7, centrifuge, air-dry and package to obtain calcium formate product, and the mother liquor is recy...
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