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Equipment and method for collecting nanoparticles in grading manner

A nanoparticle and equipment technology, which is applied in the equipment and field of classifying and collecting nanoparticles, can solve the problems of low yield, uneven particle size, complicated process control, etc., and achieve the effect of high yield, uniform particle size classification, and simple equipment structure

Active Publication Date: 2013-02-27
HUNAN GUANGGU NANO SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The above-mentioned physical method has low productivity, small output, low product purity, uneven particle size distribution, and a single variety of metal nanometers, and it is impossible to produce composite metal nanopowder materials with multiple components in proportion at any time according to needs.
Chemical methods such as: electrolysis method, microemulsion method, chemical plating reduction method, carbonyl thermal decomposition method, etc. The disadvantages of chemical methods are low output, complicated process control, difficult mass production, and certain pollution, etc.
[0003]The patent literature of CN1943924A discloses a method for preparing nanoparticles by lightning gasification of metal wires. The continuous preparation of particles, at the same time, by using different protective gases to obtain nanoparticles with high purity, solves the problems of low yield, small output, low product purity, and uneven particle size when prepared by traditional methods
[0007] (2) Due to the large specific surface area of ​​nanoparticles, when in contact with air or other media, they are easy to absorb or interact with media such as gases, resulting in adhesion and agglomeration;
[0008] (3) Due to its high surface energy and large contact interface, when the nanoparticles are exposed without modification, the growth rate of the grains is accelerated, so the particles Difficult to stay the same size
Therefore, only agglomerated and single nanoparticles can be collected during collection, and nanoparticles of different particle sizes cannot be collected in grades, resulting in single nanoparticles with low quality
At present, in the nanoparticle preparation process, there is only theoretical classification and collection by airflow, but the actual effect is not good or effective classification cannot be achieved at all.

Method used

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  • Equipment and method for collecting nanoparticles in grading manner
  • Equipment and method for collecting nanoparticles in grading manner
  • Equipment and method for collecting nanoparticles in grading manner

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Experimental program
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Effect test

Embodiment 1

[0053] see Figure 3 to Figure 7 , the equipment for classifying and collecting nanoparticles includes an ultrasonic dispersing device 7 connected in sequence by pipelines, a degaussing device 8, an automatic airflow control device 9 and a classifying collection system 10; an ultrasonic generator 18 is provided in the ultrasonic dispersing device 7; The degaussing device 8 is provided with an alternating magnetic field composed of two degaussing plates 19; the airflow inlet end of the airflow automatic control device 9 is provided with a wind speed sensor 20, and the airflow outlet end is provided with a valve connected to the damper controller 21. Damper; the classification collection system 10 includes a plurality of collectors, the top of the collector is provided with an air inlet and outlet device, and one side of the air inlet and outlet device is provided with an air intake pipe along the tangential direction of the collector port, and the top of the air inlet and outlet...

Embodiment 2

[0055] 1. Silk

[0056] According to the needs of the obtained metal nanoparticles, select high-purity suitable material metal wires, the purity of which can reach more than 95%, the length of which is 8-12 cm, and the diameter is 0.1-0.8 mm.

[0057] Install the metal wire 14 in the wire feeding device 3 , and send the metal wire into the reaction chamber 4 by rolling the upper and lower rollers in the wire feeding device 3 . Use the button to adjust the position of the wire to align with the electrode plate 16 and balance the distance between the wire and the electrode plate 16, seal the reaction chamber 4, and adjust the voltage of the high voltage to be between 25-45KV.

[0058] 2. Filling with protective gas

[0059] First turn on the vacuum pump 12 in the reaction system to evacuate the entire system to create a vacuum environment, then turn off the vacuum pump, and use the blower 11 to fill the system with protective gas until the air pressure is 1×10 ~1×10 Pa....

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Abstract

The invention discloses equipment for collecting nanoparticles in a grading manner. The equipment comprises an ultrasonic scattering device, a demagnetization device, an automatic airflow control device and a grading collection system, which are sequentially connected with one another through pipelines. The invention further provides a method for collecting the nanoparticles in the grading manner on the basis of the equipment. The method comprises the following steps that: the prepared nanoparticles are introduced into the ultrasonic scattering device to be subjected to ultrasonic scattering, then enter the demagnetization device to be subjected to demagnetization, and finally enter the grading collection system to be collected after being treated by the automatic airflow control device, thus obtaining the nanoparticles with different particle diameters. The equipment and the method provided by the invention can effectively solve the technical problem that grading collection of the nanoparticles cannot be performed well because of aggregation of the nanoparticles.

Description

technical field [0001] The invention relates to a device and a method for classifying and collecting nanoparticles. Background technique [0002] Due to the influence of the six basic physical effects of nanoparticles, nanomaterials exhibit special properties in terms of electricity, magnetism, light, catalysis, adsorption and chemical reactivity. Therefore, it can be widely used in powder metallurgy, mechanical parts manufacturing, anti-friction materials, magnetic fluids, lubricants and product development. Therefore, nanomaterials have become the focus of research and attention in the world due to their unique properties such as electricity, magnetism, heat, force, and light, and the mass production of high-quality nanopowders is a hot spot, a key point, and a difficult point. At present, the methods for preparing nano-powders of materials such as metals and alloys generally include physical methods and chemical methods. Physical methods such as mechanical alloying, sput...

Claims

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Application Information

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IPC IPC(8): B22F9/14B07B7/00
Inventor 司徒健强李强柏
Owner HUNAN GUANGGU NANO SCI & TECH
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