Preparation method of novel modified furan resin for casting
A furan resin and modification technology, applied in casting molding equipment, casting molds, manufacturing tools and other directions, can solve problems such as the unsuitability of wood board adhesives, and achieve the effects of low price, improved strength, and simple and feasible process
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Embodiment 1
[0035] Add 30g of water, 100g of sucrose and 0.1g of urea into the reaction vessel, stir at 10°C until dissolved, then add 5g of concentrated sulfuric acid, stir and raise the temperature to 60°C, react for 20h, cool down to 30°C; oxidize with 30% hydrogen Adjust the pH value to 7.5 with sodium, add 0.1 g of formaldehyde, raise the temperature at 60°C for 6 hours, and then dehydrate 5 g to obtain a brown-red viscous liquid.
[0036] According to the corresponding steps of the comparative example, under the constant conditions of steps (1) to (3), get the above-mentioned brownish red viscous liquid 5g in the step (4) to replace the 5g furfuryl alcohol in the step (4) of the comparative example (the total amount of raw materials 5% of weight), the raw materials that actually participate in the reaction are 35g furfuryl alcohol, 5g brownish-red viscous liquid and 0.85g silane coupling agent, and other conditions are constant to obtain furan resin for modified casting, and its perf...
Embodiment 2
[0038] Add 60g of water, 100g of glucose and 5g of urea into the reaction vessel, stir at 30°C until dissolved, then add 10g of concentrated nitric acid, stir and raise the temperature to 80°C, react for 4 hours, and cool down to 40°C; use 30% sodium hydroxide Adjust the pH value to 8.5, add 6g of formaldehyde, heat up to 70°C for 4 hours, and then dehydrate 80g to obtain a brown-red viscous liquid.
[0039] According to the corresponding steps of the comparative example, under the constant condition of steps (1)~(3), get the above-mentioned brownish-red viscous liquid 5g in the step (4) to replace the 10g furfuryl alcohol in the comparative example step (4) (the total amount of raw materials 10% of weight), the raw materials that actually participate in the reaction are 30g furfuryl alcohol, 10g brownish-red viscous liquid and 0.85g silane coupling agent, and other conditions are constant to obtain furan resin for modified casting, and its performance is shown in Table 1.
Embodiment 3
[0041] Add 76g of water, 100g of sucrose and 7.5g of urea into the reaction vessel, stir at 40°C until dissolved, then add 25g of concentrated hydrochloric acid, stir and raise the temperature to 84°C, react for 2 hours, and cool down to 50°C; adjust with 20% ammonia water When the pH value reached 8.5, 8g of formaldehyde was added, the temperature was raised to 95°C for 1 hour, and then 98g was dehydrated to obtain a brown-red viscous liquid.
[0042] According to the corresponding steps of the comparative example, under the constant conditions of steps (1) to (3), get the above-mentioned brownish-red viscous liquid 20g in step (4) to replace 20g furfuryl alcohol in the step (4) of the comparative example (the total amount of raw materials 20% of weight), the raw materials that actually participate in the reaction are 20g furfuryl alcohol, 20g brownish red viscous liquid and 0.85g silane coupling agent, and other conditions are constant to obtain furan resin for modified casti...
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