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Preparation method of additive for fungus polysaccharide cigarettes and application of additive in cigarettes

A technology of cigarette additive and fungus polysaccharide, which is applied in the application, tobacco, processing tobacco and other directions, can solve the problems of unsatisfactory improvement effect of smoking comfort, long operation time and low yield, etc., and achieves improvement of processing performance and sensory The effect of comfort, improved dissolution rate, and increased moisturizing properties

Active Publication Date: 2015-05-27
ZHENGZHOU TOBACCO RES INST OF CNTC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there are still some deficiencies in the various polysaccharide extraction methods commonly used at present. For example, due to the thick wall thickness of the fungus cells, the polysaccharides are difficult to diffuse out of the cells. Auxiliary extraction conditions are mild and the process is simple, but the cost of enzymes is high; microwave-assisted and ultrasonic-assisted extraction have the characteristics of short time, solvent saving, and high extraction efficiency, but it is not easy to scale up the process
[0005] At present, polyhydric substances such as glycerin, propylene glycol, and sorbitol are mainly used as humectants in my country’s cigarette industry, but the purpose of using such humectants is only to maintain the moisture content of shredded tobacco during processing and improve the processing resistance of shredded tobacco. For the maintenance of moisture content in finished cigarettes, the effect of improving smoking comfort is not ideal

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The dried fungus is subjected to impurity removal and pulverization to obtain dry fungus powder, which is added with 2 times the weight of water and soaked at room temperature for 5 hours. After soaking in water, the swollen fungus was placed at -18 °C for 12 hours, and then quickly added with hot water at 70 °C to thaw, and the amount of water added was 10 times the mass of the dry fungus powder. Adjust the temperature of the system to 45°C, add 0.5% protease by weight of dry fungus powder for 1 h. Heating to 70°C and refluxing for 5h, after stopping heating, centrifuging at 2000rpm for 40min, the supernatant was concentrated under reduced pressure to a solid content of 10%. The concentrated solution is added with 95% ethanol until the ethanol concentration of the system reaches 60%, and the precipitation is filtered, washed and dried to obtain the fungus polysaccharide.

[0026] The fungus polysaccharide is dissolved in water, uniformly sprayed on the cut tobacco acc...

Embodiment 2

[0028] The dried fungus is subjected to impurity removal and pulverization to obtain dry fungus powder, which is added with 3 times the weight of water and soaked at room temperature for 3 hours. After soaking in water, the swollen fungus was placed at -18 °C for 18 hours, and then quickly added with hot water at 80 °C to thaw, and the amount of water added was 12 times the mass of the dry fungus powder. The temperature of the system was adjusted to 50°C, and 0.7% protease by weight of dry fungus powder was added for 1.5h. Heating and heating to 80°C and refluxing for 3h, after stopping heating, centrifugation at 3000rpm for 30min, the supernatant was concentrated under reduced pressure to a solid content of 20%. The concentrated solution is added with 95% ethanol until the ethanol concentration of the system reaches 70%, and the precipitation is filtered, washed and dried to obtain the fungus polysaccharide.

[0029] The fungus polysaccharide is dissolved in water, uniformly...

Embodiment 3

[0031] The dried fungus is removed and pulverized to obtain dry fungus powder, 5 times the weight of water is added, and it is soaked at room temperature for 1 hour. After soaking in water, the swollen fungus was placed at -18°C for 24 hours, and then 90°C hot water was quickly added to thaw, and the amount of water added was 8 times the mass of the dry fungus powder. The temperature of the system was adjusted to 55°C, and 0.1% protease by weight of dry fungus powder was added for 1 h. The mixture was heated to 90°C and refluxed for 2 hours. After the heating was stopped, it was centrifuged at 4000 rpm for 10 minutes. The supernatant was concentrated under reduced pressure to a solid content of 300%. The concentrated solution is added with 95% ethanol until the ethanol concentration of the system reaches 80%, and the precipitation is filtered, washed and dried to obtain the fungus polysaccharide.

[0032] The fungus polysaccharide is dissolved in water, 0.01% of the weight of...

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PUM

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Abstract

The invention relates to a preparation method of an additive for fungus polysaccharide cigarettes and an application of the additive in the cigarettes. The preparation method is characterized in that fungus polysaccharides are prepared by taking fungus as a raw material through the following method: getting the dry fungus, removing impurities, crushing, soaking, freezing, unfreezing, deproteinizing, boiling in water, centrifugalizing, concentrating, performing ethanol precipitation, filtering and drying. The additive for the fungus polysaccharide cigarettes is added into cut tobacco of the cigarettes, so that the moisture retention performance of the cut tobacco can be increased, the miscellaneous gas and the stimulus in smoke gas can be reduced, the aftertaste is sweet, fluid can be produced in the oral cavity, and the comfort of sensory organs is obviously improved. The largest characteristic of the preparation method disclosed by the invention is that a technology of combining temperature-difference wall-breaking with enzyme process deproteinization is adopted, a simple, effective and easy-to-amplify fungus polysaccharide extraction process is established, the fungus polysaccharides are applied to the cigarettes, the original performances of the cigarettes are not changed, the original processing process of the cigarettes is not changed, the processing performances and the comfort of the sensory organs of the cigarettes are improved, and the preparation method further has actual production significance and value.

Description

technical field [0001] The invention relates to the preparation and application of additives for cigarettes, in particular to the extraction of polysaccharides from fungus and its application in cigarettes. The application of this technology does not change the existing processing technology of the cigarette, and can improve the smoking quality and sensory comfort of the cigarette. Background technique [0002] Fungus, also known as ear, cloud ear, tree chicken, wood moth, wood fungus, is a fungus that grows naturally or artificially on various rotten wood. Fungus is rich in nutrition and delicious in taste, not only has high nutritional value, but also has high medicinal value. The fungus is flat in nature and sweet in taste, and has the effects of cooling blood, promoting blood circulation, relieving pain, nourishing qi and strengthening the body. Fungus is rich in resources and rich in nutrients. In recent years, it has attracted extensive attention from scholars at hom...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/00A24B15/40
Inventor 胡有持刘珊胡军宗永立
Owner ZHENGZHOU TOBACCO RES INST OF CNTC
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