Self-propagating high-temperature rapid one-step synthesis thermoelectric material powder with nanostructure Cu2Se method
A self-propagating high-temperature, nano-structured technology, applied in the field of new energy material preparation-self-propagating high-temperature synthesis, can solve the problems of destroying the stoichiometric ratio of Cu2Se, difficult to precisely control the stoichiometric ratio of products, and influence of sample performance repeatability, etc. The effect of short time, fast response and low cost
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Embodiment 1
[0025] Self-propagating high-temperature rapid one-step synthesis of Cu with nanostructure 2 The method for Se thermoelectric material powder, its steps are as follows:
[0026] (1) Take Cu powder and Se powder as raw materials, weigh Cu powder and Se powder according to the stoichiometric ratio Cu:Se=2:1, and weigh a total of 15g. Mix the raw materials evenly in an agate mortar to obtain a mixed Powder;
[0027] (2) Put the uniformly mixed powder into a steel abrasive tool, press it into a f12mm block with a pressure of 10MPa on a tablet press, and then put it into a quartz glass tube (with an inner diameter of 17mm and an outer diameter of 20mm) , in an air atmosphere, put the bottom end of the quartz glass tube on a gas flame and heat it directly until the self-propagating reaction occurs, that is, the naked eye can see that there is a bright light at the heating end of the reactant, then stop heating, and cool naturally after the reaction is completed obtained nanostruct...
Embodiment 2
[0030] Self-propagating high-temperature rapid one-step synthesis of Cu with nanostructure 2 The method for Se thermoelectric material powder, its steps are as follows:
[0031] (1) Take Cu powder and Se powder as raw materials, weigh Cu powder and Se powder according to the stoichiometric ratio Cu:Se=2:1, and weigh the total amount to 25g. Mix the raw materials evenly in an agate mortar to obtain a mixed Powder;
[0032] (2) Press the uniformly mixed powder into a block, then put it into a quartz glass tube, vacuumize and seal it, put the vacuum-sealed quartz glass tube into a muffle furnace at 500°C and heat it until the self-propagating reaction After the reaction, the heating is stopped, and after the reaction is completed, it is naturally cooled to obtain Cu with nanostructure 2 Se thermoelectric material.
[0033] image 3 The XRD spectrum of the product that is the present embodiment obtains, as can be seen from the figure, the product obtained after the self-propag...
Embodiment 3
[0035] The difference from Example 2 is that the reactant vacuum-sealed in the quartz glass tube is placed in a 400°C muffle furnace, and a single-phase Cu is obtained through a self-propagating reaction. 2 Se compounds.
[0036] Cu prepared according to this embodiment 2 The XRD of Se powder see Figure 4 .
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