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High-sphericity nano-tetragonal barium titanate for MLCC and preparation method thereof

The application relates to high-sphericity nano tetragonal barium titanate for MLCCs and a preparation method thereof. The technical scheme is as follows: a titanium source, a dissolving agent and potassium perchlorate are mixed to obtain mixed material A; the mixed material A is heated twice under air condition, is preserved, is naturally cooled to obtain a reaction product; the reaction product is washed with distilled water I, is separated, is dried to obtain titanium dioxide powder; the titanium dioxide powder and barium oxide are mixed to obtain mixed material B; the mixed material B, ethylene glycol, pure water and an anionic surfactant are mixed to obtain a mixed solution; the mixed solution is moved to a polytetrafluoroethylene reaction kettle, is placed in a microwave heating furnace, is heated, is preserved, is naturally cooled and is filtered; the filtered product is washed with distilled water II, is separated, is dried to obtain high-sphericity nano tetragonal barium titanate for MLCCs. The product prepared by the application has high purity, high sphericity, small particle size, good dispersity and high tetragonality.
Owner:WUHAN UNIV OF SCI & TECH +1