76results about How to "High purity powder" patented technology

The invention relates to a silicon nitride powder based on catalytic nitridation and a preparation method thereof. The technical scheme is as follows: the method comprises the following steps: mixing a dispersing agent, silicon powder and distilled water in a mass ratio of 1:200:(10000-16000), stirring, and carrying out ultrasonic dispersion to obtain a suspension; adding 0.88 mol/L water-soluble chromium salt into the suspension according to the Si:Cr2O3 mass ratio of 1:(0.005-0.050) to obtain a mixed solution; adding a precipitant into the mixed solution until the pH value is 7.5-8.5, and stirring for 0.5-1 hour; carrying out vacuum filtration and vacuum drying to obtain a powder mixture; and putting the powder mixture into a tubular atmosphere furnace, heating to 1250-1400 DEG C in a nitrogen atmosphere, and keeping the temperature for 2-8 hours to obtain the silicon nitride powder based on catalytic nitridation. The method has the characteristics of low synthesis temperature, short period, simple technique and high yield, and is easy to control. The silicon nitride powder based on catalytic nitridation has the advantages of high purity and small particle size, and is partially crystal whiskers.

The invention discloses three-dimensional flower-shaped bismuth ferrite powder and a preparation method thereof. The preparation method comprises the following steps: taking Bi(nO3)3.5H2O and Fe(NO3)3.9H2O as starting materials, preparing blocky bismuth ferrite powder by adopting a hydrothermal method, then mixing the bismuth ferrite powder, a corrosive solvent, a reducing agent and a complex agent under the protective atmosphere, and obtaining three-dimensional porous bismuth ferrite flower balls by adopting a one-step corrosion method. According to the invention, a thick flaky Bi2Fe4O9 powder raw material is prepared by adopting the hydrothermal method, grains are uniform in size and shape and are better in dispersibility, a corrosion technology is adopted, preparation technological operation is simple, and the period is short; and the prepared flower-shaped bismuth ferrite has the diameter being about 1-2mu m, sizes are uniform, a specific surface area is relatively large due to a porous structure, and performances of all the aspects are respectively improved.

A process for preparing sulfide nano-particles includes such steps as preparing the solution of metal salt, adding quaternary ammonium salt, dripping the solution of sodium sulfide in it to generate deposit, filter, water washing, removing the ions of impurities, drying and calcining.

The invention discloses a clean production method for high-purity cobaltosic oxide powder. The method comprises the following steps: using metal cobalt as an electrolytic anode, using soluble cobalt salt as electrolyte main salt and adding additives; adopting an electrochemical method to prepare a cobaltosic oxide precursor sediment; and then, drying and calcining the precursor sediment to obtain the cobaltosic oxide powder. The cobaltosic oxide powder produced by the method and the process can achieve the purity more than 99.7 percent, no additional precipitator is needed in the whole technological process, the added additives are all easy to wash without decomposition, and electrolyte and washing water can be recycled so as to avoid discharging sewage and generating waste gas. The method can adjust and control the appearance and the grain diameter distribution of the cobaltosic oxide powder by controlling the composition of the electrolyte, the cathode current concentration, the electrodeposition time and the calcining temperature and has the advantages of high product quality, simple production procedures, energy saving, environmental protection, and the like.

The present invention provides one waste copper containing acid solution recovering and utilizing process in saccharin sodium production. The waste copper containing acid solution recovering and utilizing process includes filtering to eliminate suspended organic matter, oxidizing the filtrate with mixed oxidant of sodium hypochlorite and potassium hypermanganate to eliminate low boiling point organic matter, decompression distilling the solution in vacuum to obtain dilute hydrochloric acid solution, further extraction and concentrating distillation to obtain hydrochloric acid solution of 30 % concentration, burning residue after decompression distilling to eliminate organic matter and obtain high purity copper sulfate and powder of other inorganic salts. The said process can recover the useful matter from waste acid solution and avoid environmental pollution effectively.

The invention relates to a method for synthetizing Ti3SiC2 high-purity powder. The method comprises the following steps: 1) proportioning: selecting Ti powder, SiC powder and TiC powder as raw materials and Al powder as a synthesizing accelerator wherein the molar ratio of Ti to SiC to TiC to Al is (4-4.1): (2-2.1): (1-1.1): (0.2-0.3); mixing the Ti powder, SiC powder, TiC powder and Al powder to obtain a mixture; 2) performing wet grinding on the mixture, sieving, washing to obtain a mixed suspension; 3) standing the mixed suspension, pouring out the supernatant, performing vacuum drying to obtain pretreated mixed powder; and 4) placing the pretreated mixed powder in a vacuum furnace to heat to 1250-1300 DEG C in a heating rate of 15-20 DEG C/min, treating under the condition that the vacuum degree is 1*10<-3>-1*10<-2>Pa, keeping the temperature for 1-2 hours, and obtaining the Ti3SiC2 high-purity powder under the condition that the furnace temperature is reduced to the room temperature. The Ti3SiC2 powder synthetized by the method has high purity and does not require purification treatment; the process is greatly simplified, the technological parameters are stable, the cost is low, the growth of grains is good; and the method is very suitable for mass production.

This invention relates to a synthetic method of aluminium carbide titanium ceramic powder. The invention takes TiH2 powder, Al powder and TiC powder as raw material, add Sn as accessory ingredient, dyr mix the raw materials acoording to mol ratio of TiH2:TiC:Al:Sn=1:1:1:0.1 for 10 hours, execute piece under 30 to 50 pressure, then put at high temperature furnace, under vacuum atmosphere rise the furnace temperature to 1350 to 1550 deg by rate of 15 to 40 deg per minute, holding time for 5 to 15min, execute low cost high-purity Ti3AlC2 powder.

The invention relates to Ti3AlC2 powder and a preparation method thereof. The preparation method comprises the steps: taking titanium powder, aluminum powder and graphite as reaction materials, takingsodium chloride and potassium chloride as molten salt media, performing ball milling on the reaction materials and the molten salt media, putting a ball-milled ball abrasive into an aluminum oxide crucible, putting the aluminum oxide crucible into a thermal insulation structure sagger, filling a gap between the thermal insulation structure sagger and the aluminum oxide crucible with silicon carbide powder, and putting the thermal insulation structure sagger into a microwave oven; sequentially heating to 440-460 DEG C, 590-610 DEG C and 900-1200 DEG C at three heating rates in an argon atmosphere, carrying out heat preservation for 5-60 min under a condition of the temperature of 900-1200 DEG C, and carrying out furnace cooling to room temperature; and finally, grinding, washing with water, carrying out suction filtration and drying to obtain the Ti3AlC2 powder. The method has the characteristics of high raw material utilization rate, short production period, low energy consumption andhigh production efficiency, and the prepared Ti3AlC2 powder is high in purity and suitable for mass production.

The invention provides a method for preparing nano ZnO by virtue of metallurgy. The method comprises the following steps of: reducing zinc ores by adopting hydrogen to form a zinc liquid, evaporating the zinc liquid at high temperature, and then introducing water vapor for reaction to form ZnO powder and hydrogen which is recycled. According to the method, not only can nano ZnO with good quality be prepared, but also the hydrogen can be generated and recycled. The ZnO powder prepared by the method is high in purity and uniform in particle size; and the cost of the whole method is low, the use equipment is simple, the industrial production is easy, and the method is a novel and high-efficiency technology for preparing the nano ZnO powder and recycling the hydrogen.

The invention relates to a processing method for increasing blueberry anthocyanidin content and purity. The processing method comprises the following steps: accurately weighting 20g of blueberry fresh fruit, washing by distilled water, air drying the moisture on the surface, crushing, homogenating, placing in a triangular flask, taking 2% of hydrochloric acid-methanol as an extraction solvent, setting the ratio of the solvent to fresh fruit as 5-20, extracting the pH value as 1.5-2.5, wherein cellulase accounts for 1-4% of the fresh fruit, and the enzymatic hydrolysis temperature is 40-70 DEG C, and performing an enzymatic hydrolysis reaction for 1 hour. The water-bath extraction is completed and then pumping filtration is carried out, the obtained filtrate enables rotary evaporation, and is performed with freeze drying to obtain a blueberry anthocyanidin crude extract. The blueberry anthocyanidin content is 5.15-5.65mg/100g through high performance liquid chromatography determination. The blueberry anthocyanidin content is 3.65mg/100g after the blueberry anthocyanidin is treated by a traditional solvent adding extraction method. The method for processing blueberry anthocyanidin has the advantages of simple operation, low cost, less pollution and high product content. the loss of blueberry anthocyanidin active components is far lower than that of the blueberry anthocyanidin active components by a solvent adding processing technology, and the purity of the obtained blueberry anthocyanidin powder is far higher than that of the blueberry anthocyanidin product on shelf.

The invention relates to a solid-phase preparation method for beta-eucryptite powder. The preparation method comprises the following steps: 1) weighing lithium carbonate, silica and alpha-alumina according to equimolar proportion; 2) subjecting the raw materials weighed in the step 1) to grinding and mixing in a rapid grinding device; and 3) filling an alumina saggar with the raw materials ground and mixed in the step 2), placing the alumina saggar in a high-temperature furnace and carrying out calcining so as to obtain desired beta-eucryptite powder. The preparation method is simple in process, low in equipment requirement, nontoxic and pollution-free; the prepared beta-eucryptite powder has high purity; and the preparation method is suitable for batch production.

The invention relates to a preparation method of special magnesium oxide for grain-oriented silicon steel sheet, belonging to the technical field of the preparation special magnesium oxide. The methodcomprises the following steps: reacting magnesium compound solution with the mixed solution of sodium carbonate and sodium hydroxide at a temperature to prepare a mixture of intermediate product containing magnesium carbonate and magnesium hydroxide, filtrating, washing, drying, calcining at high temperature, and grinding to obtain the special magnesium oxide for grain-oriented silicon steel sheet. The method has the advantages that the raw material is accessible, the cost is low, the production process is simple, the facility request is low, the method is applicable to industrialized production; the intermediate product is easy for separation and purification and is easy to wash, the washing loss of the product is low, the product yield is high; the product is special magnesium oxide powder, the powder has high purity, the grain size is small, and the average grain size is 1-2mu m and has a certain distribution range. The method is especially suitable for the preparation of special magnesium oxide for grain-oriented silicon steel sheet.

The invention discloses a method for preparing AlN powder. The method includes first dissolving an aluminum source and a nitrogen source completely in a solvent according to the Al:N molar ratio of 1:1-1:35, mixing evenly, drying the solvent by evaporating, roasting an obtained solid mixture at 500-1000 DEG C for 1-9h in a roasting atmosphere, and then decarburizing the mixture at 200-750 DEG C for 1 to 5h in an air atmosphere to obtain the high-purity AlN powder. The aluminum source is aluminum chloride hydrate, aluminum lactate, aluminum glycinate, aluminum stearate and the like; the nitrogen source is guanidine hydrochloride, guanidine acetate, chitosan, 1,10-phenanthroline; the solvent is any one of deionized water, methanol, ethanol, ethyl acetate, acetone, diethyl ether, benzene andtoluene; the roasting atmosphere is one or two of nitrogen, ammonia, argon and helium. Compared with the conventional AlN preparation method, the method has the advantages of wide reactant range, environmentally-friendly process, simple operation, high product purity and low cost.

The invention relates to an aquatic product deep processing technology, and specifically relates to clam concentrated liquid or clam powder, and a production method thereof. According to the invention, clam steaming and boiling liquid obtained during a clam processing process is adopted as a raw material; impurities are removed by micro-filtration; and salt and part of water content are removed by ultra-filtration or nano-filtration, such that the clam concentrated liquid is obtained. Measured according to standard, every 100g of the concentrated liquid comprises the components of: 5-30g of protein, 0.5-5g of fat, 2-15g of total sugar, 5-20g of an ash content, and balance of water. The clam concentrated liquid is subjected to vacuum lyophilization or spray-drying, such that crude clam powder is obtained; the crude clam powder is crushed by using a supersonic jet mill, such that clam powder is obtained. Every 100g of the clam powder comprises the components of: 20-65g of protein, 2-15g of fat, 3-20g of total sugar, 5-20g of an ash content, and 3-10g of water.

The invention relates to a synthesis method of sic ceramic powder at ordinary pressure. The invention is made from the following materials that are TiH2 powder, Si powder, and TiC powder, and the using of Al which is used as reaction promoter. The materials, according to a certain mole ratios of Ti: Si: TiC: Al of 1:1: (1.8-2): (0.15-0.25), are mixed dryly together for 10 hours, and then are compacted into briquetting under the pressure of 30-50 MPa. Then the briquetting is put into high temperature furnace at vacuum condition. Next in a heating increasing rate of 15-50 DEG C/min, the temperature in furnace is increased to 1300-1550 DEG C and is kept for 5-15min, then the Ti3SiC2 powder of high purity and low cost is obtained. The invention is characterized by short synthesis time of Ti3SiC2 powder, high purity, low cost, simple equipment, and stable technical parameter, and being suitable for large scale production.

The invention relates to a batch preparation method of pentatitanium trisilicate intermetallic compound powder. Si powder and Ti powder are weighed according to a mole ratio of 3: 5 as sintering raw materials; a Ti5Si3 compound is synthesized by adopting a vacuum sintering process; the sintering process comprises the following steps: the Si powder and the Ti powder, uniformly mixed, are put in a vacuum furnace, are heated to 1350-1450 DEG C for insulation, and are cooled to the room temperature along with the furnace; the sintering materials are added in anhydrous ethanol, and are put in a ball milling tank; Ar gas is used as shielding gas; the sealed ball milling tank is put in a high-energy planet ball mill; a wet ball milling method is used for refining; and vacuum drying and grinding are performed on obtained ball milling pulp to pass through a sieve of 130 meshes to obtain Ti5Si3 powder. The method overcomes the defects of easy generation of pollutions, complex machining process,low yield and the like in a casting method, a powder press sintering method, a quick solidification method and a self-propagating combustion method. No by-product is generated in the reaction process;the powder purity is high; meanwhile, the chemical ratios of products can be precisely controlled; the energy consumption is low; the particle sizes of the products are fine and uniformly distributed; the activity is high; the products can be prepared in batches; no pollution is generated; and the cost is reduced.

The invention discloses a method for preparing magnesium-aluminum spinel nano particle powder, which comprises the following steps of: preparing water soluble aluminate into an aqueous solution with the Al3<+> concentration of 0.05-1mol/L; then adding alkali; filtering aluminium hydroxide; after washing, carrying out drying treatment and grinding into fine powder in 200-1,000 meshes; adding the ground fine powder into a magnesium sulfate aqueous solution; after fully stirring, carrying out drying treatment to obtain the mixed powder of aluminium hydroxide and magnesium sulfate; calcining the mixed powder at 800-950 DEG C for 2-5 hours; and after washing a calcined product with water and removing magnesium sulfate, carrying out drying treatment under the condition of 80-100 DEG C. The invention discloses an environmental-friendly and energy-saving method for producing high-purity agglomeration-free magnesium-aluminum spinel nano particle powder at an industrial scale.