A method and apparatus for detecting aluminum
carbide content includes a right-angle tube I connected to a round-bottom flask via a rubber stopper I at its inlet. One end of the rubber tube I is connected to one port of a three-way valve, and the other two ports of the three-way valve are connected to rubber tubes II and III, respectively. The other end of the rubber tube II is connected to the gas inlet of a gas chromatograph. The other end of the rubber tube III is connected to the inlet of the right-angle tube II. The outlet of the right-angle tube II, a
thermometer, and the inlet of the right-angle tube III are all embedded in the rubber stopper II and installed at the mouth of a specially designed measuring cylinder. The outlet of the right-angle tube III is connected to the inlet of the right-angle tube IV via a rubber tube IV. The outlet of the right-angle tube IV, along with a
glass tube, is embedded in the rubber stopper III and installed at the mouth of a conical flask. By measuring the gas volume and composition sequentially through the three-way valve, the aluminum
carbide content in the sample is determined using a
function model. This allows for
direct observation of changes during the detection process, effectively reducing operational errors and improving the accuracy of the detection results.