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Aluminium nitride-based multi-element nano-composite ceramic die material and preparation method thereof

A nano-composite and ceramic mold technology, applied in the field of ceramic mold materials, can solve the problems of nano-composite performance and price advantages that cannot be fully utilized in the mold field, and achieve improved mechanical properties and usability, good comprehensive mechanical properties, good The effect of overall performance

Active Publication Date: 2014-11-26
辽宁跨克石油装备有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] From the existing research, it can be seen that the performance and price advantages of nanocomposites, especially nanocomposite ceramics, have not been fully utilized in the field of molds.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] An aluminum nitride-based multi-component nanocomposite ceramic mold material, the raw materials in parts by weight are: 60 parts of aluminum nitride, 10 parts of aluminum carbide, 15 parts of silicon boride, 2 parts of scandium oxide, 4 parts of neodymium oxide, chromium 2 parts, 1 part of tungsten, and 1 part of nickel; all the above-mentioned raw materials are made of nano-scale powder, wherein the particle size of aluminum nitride is 10-100 nanometers, and the particle size of aluminum carbide and silicon boride is 1-10 nanometers. Other particle sizes are 1-100 nanometers; the preparation method is based on aluminum nitride, adding aluminum carbide and silicon boride as a reinforcing phase, using scandium oxide and neodymium oxide as stabilizers, and using chromium, tungsten and nickel as The sintering aid is sintered by hot pressing; the specific preparation steps are as follows:

[0025] Step 1: taking all the above-mentioned raw materials according to parts by w...

Embodiment 2

[0033] An aluminum nitride-based multi-component nanocomposite ceramic mold material, the raw materials in parts by weight are: 70 parts of aluminum nitride, 15 parts of aluminum carbide, 20 parts of silicon boride, 4 parts of scandium oxide, 6 parts of neodymium oxide, and 3 parts of chromium , 2 parts of tungsten and 2 parts of nickel; all of the above raw materials are made of nano-scale powder, of which the particle size of aluminum nitride is 10-100 nanometers, the particle size of aluminum carbide and silicon boride is 1-10 nanometers, and the other The particle size is 1-100 nanometers; the preparation method is based on aluminum nitride, adding aluminum carbide and silicon boride as a reinforcing phase, using scandium oxide and neodymium oxide as stabilizers, and using chromium, tungsten and nickel as sintering aids The agent is formed by hot pressing and sintering; the specific preparation steps are as follows:

[0034] Step 1: taking all the above-mentioned raw mater...

Embodiment 3

[0042] An aluminum nitride-based multi-component nanocomposite ceramic mold material, the raw materials in parts by weight are: 80 parts of aluminum nitride, 20 parts of aluminum carbide, 25 parts of silicon boride, 6 parts of scandium oxide, 8 parts of neodymium oxide, and 4 parts of chromium , 3 parts of tungsten and 3 parts of nickel; all the above raw materials are made of nano-scale powder, wherein the particle size of aluminum nitride is 10-100 nanometers, the particle size of aluminum carbide and silicon boride is 1-10 nanometers, and the other The particle size is 1-100 nanometers; the preparation method is based on aluminum nitride, adding aluminum carbide and silicon boride as a reinforcing phase, using scandium oxide and neodymium oxide as stabilizers, and using chromium, tungsten and nickel as sintering aids The agent is formed by hot pressing and sintering; the specific preparation steps are as follows:

[0043] Step 1: taking all the above-mentioned raw materials...

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PUM

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Abstract

The invention discloses an aluminium nitride-based multi-element nano-composite ceramic die material and a preparation method thereof. The material comprises the following raw materials in parts by weight: 60-80 parts of aluminium nitride, 10-20 parts of aluminium carbide, 15-25 parts of silicon boride, 2-6 parts of scandium oxide, 4-8 parts of neodymium oxide, 2-4 parts of chromium, 1-3 parts of tungsten and 1-3 parts of nickel, wherein nanoscale powder of all the materials is adopted; the grain size of aluminium nitride is 10-100 nanometers; the grain sizes of aluminium carbide and silicon boride are 1-10 nanometers; the grain sizes of the other raw materials are 1-100 nanometers. The preparation method is characterized by using aluminium nitride as the matrix, adding aluminium carbide and silicon boride as reinforcing phases, scandium oxide and neodymium oxide as stabilizing agents and chromium, tungsten and nickel as sintering aids and carrying out hot pressed sintering on the materials, thus preparing the material. A die has strong ageing and defect resistance, good comprehensive mechanical properties and excellent antifriction and wear resistance properties.

Description

technical field [0001] The invention relates to a ceramic mold material, in particular to an aluminum nitride-based multi-element nanocomposite ceramic mold material and a preparation method thereof. Background technique [0002] Ceramic cutting tools have high hardness and wear resistance, and exhibit excellent cutting performance in high-speed cutting and dry cutting, and are a class of cutting tool materials with great development prospects. However, most of the currently used ceramic tool materials are limited to micro-composite ceramics, and the mechanical properties of the materials, especially the strength and toughness, still need to be further improved. According to the Hall-petch relationship: the smaller the grain size, the higher the strength of the ceramic material. Therefore, the research and development of nano-modified and nano-micro composite ceramic tool materials will be one of the main directions for the development of tool materials in the future. [0...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/582C04B35/622
Inventor 韩巧李孝君
Owner 辽宁跨克石油装备有限公司
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