Multifunctional softener and preparation method for same

A multi-functional, fabric softener technology, used in textiles, papermaking, fiber processing, etc., can solve the problems of high parameter control ability, complex configuration process, difficult production and application, etc., and achieve good washing durability, preparation process Simple process, good bioactive effect

Active Publication Date: 2013-09-25
JIANGSU GOLDSUN TEXTILE SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The patent application No. 200710011759.X "An Antibacterial Fabric Finishing Solution Containing Chitosan, Preparation Method and Its Application Method" provides a fabric finishing solution containing chitosan, which is composed of chitosan, acetic acid, epoxy chlorine Composed of propane and water, it is soluble under weakly acidic conditions and has good antibacterial effect, but after compounding with non-ionic surfactants such as other softeners, chitosan will precipitate under neutral or alkaline conditions, thus the antibacterial function disappears
[0007] The patent "Water-Soluble Chitosan Quaternary Ammonium Salt Antibacterial Finishing Agent and Its Preparation and Application" with the application number of 200910200566.8 is to introduce hydrophilic groups into the amino groups of chitosan, so that it can be dissolved in water, but its configuration process is complicated , and the requirements for the control ability of various parameters in the process are relatively high, so it is difficult to carry out industrial production and application

Method used

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  • Multifunctional softener and preparation method for same

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] A preparation method for a multifunctional fabric softener, comprising the steps of:

[0038] One, the preparation of water-soluble chitosan

[0039] Stir chitosan and isopropanol to reflux, heat in a water bath, raise the temperature to 30°C, slowly add the modifier dimethyl sulfate dropwise; after stirring evenly, raise the temperature to 70°C, and react for 12 hours; after the reaction is completed, stop heating And the solution was cooled, filtered with suction, and distilled under reduced pressure to obtain rough water-soluble chitosan. Wash with ethanol-acetone solution, filter with suction, and dry to obtain refined water-soluble chitosan.

[0040] Among them, the particle size of chitosan is 80 mesh, the degree of deacetylation is 85%; the mass ratio of chitosan to isopropanol is 1:10; the molar ratio of chitosan to modifier is 1:3; The volume ratio of ethanol to acetone is 0.4:1.

[0041] 2. Compounding of compound emulsifier

[0042] Highly purified surfac...

Embodiment 2

[0056] One, the preparation of water-soluble chitosan

[0057] Chitosan and isopropanol were stirred and refluxed, heated in a water bath, and the temperature was raised to 50°C, and the modifier 3-epoxypropyltrimethylammonium chloride was slowly added dropwise; after stirring evenly, the temperature was raised to 80°C, and the reaction was carried out for 10 hour; after the reaction was completed, stop heating and cool the solution, filter it with suction, and carry out distillation under reduced pressure to obtain the rough body of water-soluble chitosan. Wash with ethanol-acetone solution, filter with suction, and dry to obtain refined water-soluble chitosan.

[0058] Among them, the particle size of chitosan is 90 mesh, the degree of deacetylation is 90%; the mass ratio of chitosan to isopropanol is 1:30; the molar ratio of chitosan to modifier is 1:5; The volume ratio of ethanol to acetone is 1:1.

[0059] 2. Compounding of compound emulsifier

[0060] The mass fractio...

Embodiment 3

[0072] One, the preparation of water-soluble chitosan

[0073] Mix chitosan and isopropanol, stir and reflux, heat in a water bath, raise the temperature to 60°C, slowly add the modifier 3-chloro-2-hydroxypropyltrimethylammonium chloride dropwise; after stirring evenly, raise the temperature to 90°C , reacted for 8 hours; after the reaction was completed, the heating was stopped and the solution was cooled, suction filtered, and vacuum distillation was carried out to obtain the rough water-soluble chitosan. Wash with ethanol-acetone solution, filter with suction, and dry to obtain refined water-soluble chitosan.

[0074] Among them, the particle size of chitosan is 100 mesh, and the degree of deacetylation is 95%; the mass ratio of chitosan to isopropanol is 1:20; the molar ratio of chitosan to modifier is 1:8; The volume ratio of ethanol to acetone is 1.8:1.

[0075] 2. Compounding of compound emulsifier

[0076] Highly purified surfactants usually form loose interfacial f...

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Abstract

The invention provides a multifunctional softener and a preparation method for the same. The multifunctional softener is composed of amino silicon oil, a compound emulsifier, water-soluble chitosan and water, wherein amino silicon oil is added in the compound emulsifier, and the mass ratio of the amino silicon oil to the compound emulsifier is 1:(0.2-0.8); then the water-soluble chitosan is added, and the added amount is 1-8% of the mass of the mixed solution of the amino silicon oil and the compound emulsifier; finally, water is added, and the mass of water is 10-50% of the total mass of the mixed solution aforementioned. The preparation method comprises the following steps of: preparation for the water-soluble chitosan, preparation for the compound emulsifier, and preparation for the multifunctional fabric softener. The multifunctional integrated softener obtained after compounding has all the excellent characteristics of modified chitosan on the basis of a soft function. Compared with the existing softener with an anti-bacterial function, the preparation process flow is simple, a complex configuration process is not required, and industrialized production is easy to realize.

Description

[0001] technical field [0002] The invention belongs to the technical field of textile post-finishing auxiliaries, and in particular relates to a multifunctional fabric softener and a preparation method thereof. [0003] Background technique [0004] With the development of textile technology, more and more textiles can be processed through different finishing processes to make them have corresponding functions, thereby increasing the added value of textiles. Soft finishing of all kinds of textiles, especially bedding textiles, is a post-finishing process that must be carried out. Therefore, the selection of softeners is very important. However, consumers require textiles to have antibacterial and anti-mite related functions on the basis of satisfying the hand feel. In order to meet these functions, some products separately add antibacterial agents in the finishing process for antibacterial finishing, which is complicated and costly. However, most of the softeners on the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/643D06M15/03D06M15/53D06M13/224D06M13/463D06M13/256C08B37/08
Inventor 李海乐陈红霞陆鹏丁可敬
Owner JIANGSU GOLDSUN TEXTILE SCI & TECH
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